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Determina??o de umidade em café cru usando espectroscopia NIR e regress?o multivariadaDOI: 10.1590/S0101-20612008000100003 Keywords: moisture determination, coffee, infrared spectroscopy, multivariate regression. Abstract: near infra-red reflectance (nir) spectroscopy was used to measure the moisture content in raw coffee. different models using partial least squares (pls) with data pre-processing were used. regression models were built with 157 spectra of the samples of raw coffee collected using a near infrared spectrometer with an accessory of diffuse reflectance, between 4500 and 10000 cm-1. the original nir spectra went through different transformations and mathematical pre treatments, such as the kubelka-munk transformation; multiplicative signal correction (msc); spline smoothing and movable average, and the data were scaled by variance. the regression model permitted the determination of the moisture content of the raw coffee samples with a standard error of calibration (sec) = 0.569 g.100 g -1; standard error of validation = 0.298 g.100 g -1; correlation coefficient (r) 0.712 and 0.818 for calibration and validation, respectively, and average relative error of 4.1% for validation samples.
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