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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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Ni(II),Co(II),andCu(II)complexesincorporating2-pyrazinecarboxylicacid:Synthesis,characterization,electrochemicalevaluation,andcatalyticactivityforthesynthesisof2H-indazolo[2,1-b]phthalazine-triones
DOI: 10.1016/S1872-2067(14)60318-1, PP. 1101-1108
Keywords: 2-Pyrazinecarboxylatecomplexe,ONbidentateligand,X-raycrystalstructure,Cyclicvoltammetry,2H-indazolo[2,1-b]phthalazine-triones
Abstract:
？Threecomplexescontaining2-pyrazinecarboxylate(pzca-),including[Ni(pzca)2(H2O)2],[Co(pzca)2(H2O)2],and[Cu(pzca)2(H2O)2],havebeensynthesizedandcharacterizedusingphysicochemicalandspectroscopicmethods.Furthermore,thestructureofeachcomplexwasdeterminedbysingle-crystalX-raydiffraction.Allthreecomplexeshaveanoctahedralgeometry,wherethemetalionchelatedbytwocarboxylateoxygens,twonitrogenatomsbelongingtopyrazinicacidmolecules,andtwooxygenatomsoftwowatermolecules.Thecatalyticactivitiesofthesecomplexeswerealsoinvestigatedinthegreensynthesisof2H-indazolo[2,1-b]phthalazine-trionesbythereactionofhydrazinehydratewithanarylaldehyde,phthalicanhydride,anddimedoneinaceticacid.
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