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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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Selectiveoxidationofalcoholsovercopperzirconiumphosphate
DOI: 10.1016/S1872-2067(14)60096-6, PP. 1529-1533
Keywords: Copperzirconiumphosphate,Selectiveoxidation,Solidcatalyst,Alcohol
Abstract:
？Thecatalyticactivityofcopperzirconiumphosphate(ZPCu)intheselectiveoxidationofalcoholstotheircorrespondingketonesoraldehydes,usingH2O2asanoxidizingagent,wasstudied.Theoxidationreactionwasperformedwithoutanyorganicsolvent,phase-transfercatalyst,oradditive.Stericfactorsassociatedwiththesubstratesinfluencedthereaction.ThecatalystwascharacterizedusingX-raydiffraction,inductivelycoupledplasmaatomicemissionspectroscopy,energy-dispersiveX-rayspectroscopy,andscanningelectronmicroscopy.Itwasshownthattheinterlayerdistanceincreasedfrom0.74to0.80nmandthecrystallinitywasreducedafterCu2+intercalationintothelayers.Thiscatalystcanberecoveredandreusedthreetimeswithoutsignificantlossofactivityandselectivity.
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