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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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SynthesisofNickelHexacyanoferrateNanoparticlesandTheirPotentialasHeterogeneousCatalystsfortheSolvent-FreeOxidationofBenzylAlcohol
DOI: 10.1016/S1872-2067(10)60292-6, PP. 1844-1849
Keywords: hexacyanoferratenanoparticle,heterogeneouscatalyst,benzylalcohol,benzaldehyde
Abstract:
？Nickelhexacyanoferratenanoparticlesweresynthesizedandcharacterizedusingelementalanalysis,thermalanalysis,infraredspectroscopy,andX-raydiffraction.AFE-SEMimageofthenickelhexacyanoferrateshowedthatitconsistsofnearlysphericalparticleswithsizesrangingfrom30to70nm.Thesynthesizedmaterialwasfoundtobeaheterogeneouscatalystusefulforthesolvent-freeoxidationofbenzylalcoholwithH2O2asanoxidant.A36%conversionofbenzylalcoholtobenzaldehydewasachievedunderoptimizedreactionconditionsusingspecificparameterssuchastheamountofcatalyst,thetemperature,thebenzylalcoholtoH2O2molarratio,andthereactiontime.
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