|
OALib Journal期刊
ISSN: 2333-9721
费用:99美元
|
|
|
|
qualitativeandquantitativeatr-ftiranalysisanditsapplicationtocoalcharofdifferentranks
, PP. 129-137
Keywords: qualitative,quantitative,ft-ir,coalchar
Abstract:
?thispaperanalyzesthecoaltocharstagesofcharformationofsixcoalsofdifferentranksbyusingfouriertransforminfraredcoupledwithattenuatedtotalreflectance(atr-ftir).thecharswereobtainedbycoalpyrolysiscarriedoutattemperaturerangeof450~700.thedataobtainedshowsthepragmaticdisappearanceofthealiphatichydrogencontentwithincreasingcharformationtemperature.numericalevaluationofthespectraenabledthedeterminationofaromaticity,fa.thearomaticitywasfoundtobebetween0.66~0.79forlignite,0.75~0.90forsub-bituminous,0.84~1.00forlowvolatilebituminous,0.83~1.00forhighvolatilebituminous,0.94~1.00forsemi-anthracite,and0.97~1.00foranthraciterespectively.withincreasingrankofcoalsamples,spectraexhibitrisingaromaticityandenhancedcondensationofaromaticrings,whereasthealiphaticchainlengthsdecrease.
References
| [1] | wilsonma,vassalloam.developmentsinhigh-resolutionsolid-state13cnmrspectroscopyofcoals[j].orggeochem,1985,8(5):299-312.
|
| [2] | mathewsjp,sharmaa.thestructuralalignmentofcoalandtheanalogouscaseofargonneupperfreeportcoal[j].fuel,2012,95(5):19-24.micro-ftirspectroscopy[j].intjcoalgeol,2012,104(12):22-33.
|
| [3] | taghieimm,hugginsfe,shahn,huffmangp.insitux-rayabsorptionfinestructurespectroscopyinvestigationofsulfurfunctionalgroupsincoalduringpyrolysisandoxidation[j].energyfuels,1992,6(3):293-300.
|
| [4] | guedesa,valentimb,prietoac,noronhaf.ramanspectroscopyofcoalmaceralsandfluidizedbedcharmorphotypes[j].fuel,2012,97(6):443-449.
|
| [5] | linx,wangc,idetak,miyawakij,nishiyamay,wangy,yoons,mochidai.insightsintothefunctionalgrouptransformationofachinesebrowncoalduringslowpyrolysisbycombiningvariousexperiments[j].fuel,2014,118(15):257-264.
|
| [6] | machadoas,mexiasas,vilelaacf,osorioe.studyofcoal,charandcokefinesstructuresandtheirproportionsintheoff-gasblastfurnacesamplesbyx-raydiffraction[j].fuel,2013,114(12):224-228.
|
| [7] | orrego-ruizja,cabanzor,mejía-ospinoe.studyofcolombiancoalsusingphotoacousticfouriertransforminfraredspectroscopy[j].intjcoalgeol,2011,85(3/4):307-310.
|
| [8] | sobkowiakm,painterpa.acomparisonofdriftandkbrpelletmethodologiesforthequantitativeanalysisoffunctionalgroupsincoalbyinfraredspectroscopy[j].energyfuels,1995,9(2):359-363.
|
| [9] | liz,frederickspm,rintoull,wardcr.applicationofattenuatedtotalreflectancemicro-fouriertransforminfrared(atr-ftir)spectroscopytothestudyofcoalmacerals:examplesfromthebowenbasin,australia[j].intjcoalgeol,2007,70(1/3):97-94.
|
| [10] | cookene,fullerom,gaikwadrp.ft-i.r.spectroscopicanalysisofcoalandcoalextracts[j].fuel,1986,65(9):1254-1260.
|
| [11] | edreisema,luog,yaoh.investigationsofthestructureandthermalkineticanalysisofsugarcanebagassecharduringnon-isothermalco2gasification[j].janalapplpyrolysis,2014,107:107-115.
|
| [12] | bishopan,kearsleyat,patiencerl.analysisofsedimentaryorganicmaterialsbyscanningelectronmicroscopy:theapplicationofbackscatteredelectronimageryandlightelementx-raymicroanalysis[j].orggeochem,1992,18(4):431-446.
|
| [13] | lul,sahajwallav,kongc,harrisd.quantitativex-raydiffractionanalysisanditsapplicationtovariouscoals[j].carbon,2001,39(12):1821-1833.
|
| [14] | radlinskiap,busbridgetl,grayema,blachtp,cooksondj.smallanglex-rayscatteringmappingandkineticsstudyofsub-criticalco2sorptionbytwoaustraliancoals[j].intjcoalgeol,2009,77(1/2):80-89.
|
| [15] | kelemensr,georgegn,gorbatyml.directdeterminationandquantificationofsulphurformsinheavypetroleumandcoals[j].fuel,1990,69(8):939-944.
|
| [16] | tseleva,ivanovin,lavriknv,belianinova,jesses,mathewsjp,mitchellgd,kalininsv.mappinginternalstructureofcoalbyconfocalmicro-ramanspectroscopyandscanningmicrowavemicroscopy[j].fuel,2014,126(6):32-37.
|
| [17] | charlandjp,macpheeja,girouxl,pricejt,khanma.applicationoftg-ftirtothedeterminationofoxygencontentofcoal[j].fuelprocesstechnol,2003,81(3):211-221.
|
| [18] | cheny,mastalerzm,schimmelmanna.characterizationofchemicalfunctionalgroupsinmaceralsacrossdifferentcoalranksvia
|
| [19] | dunw,guijianl,ruoyus,xiangf.investigationofstructuralcharacteristicsofthermallymetamorphosedcoalbyftirspectroscopyandx-raydiffraction[j].energyfuels,2013,27(10):5823-5830.
|
| [20] | panglsk,vassalloam,phong-anantd,wilsonma.astudyofslaginlaboratory,pilotandcommercialscalefurnacesusingftirmicroscopy,electronmicroscopyandnmrspectroscopy[j].fuelprocesstechnol,1993,33(1):13-32.
|
| [21] | sharmaa,kyotanit,tomitaa.anewquantitativeapproachformicrostructuralanalysisofcoalcharusinghrtemimages[j].fuel,1999,78(10):1203-1212.
|
| [22] | saucyda,simkosj,lintonrw.comparisonofphotoacousticandattenuatedtotalreflectancesamplingdepthsintheinfraredregion[j].analchem,1985,57(4):871-875.
|
| [23] | thomassonj,coinc,kahramanh,frederickspm.attenuatedtotalreflectanceinfraredmicrospectroscopyofcoal[j].fuel,2000,79(6):685-691.
|
| [24] | strydomca,buntjr.,schoberthh,raghoom.changestotheorganicfunctionalgroupsofaninertiniterichmediumrankbituminouscoalduringacidtreatmentprocesses[j].fuelprocesstechnol,2011,92(4):764-770.
|
| [25] | caimf,smartrb.comparisonofsevenwestvirginiacoalswiththeirn-methyl-2-pyrrolidinone-solubleextractsandresidues.1.diffusereflectanceinfraredfouriertransformspectroscopy[j].energyfuels,1994,8(2):369-374.
|
| [26] | gloverg,vanderwalttj,glasserd,prinsloonm,hildebrandtd.driftspectroscopyandopticalreflectanceofheat-treatedcoalfromaquenchedgasifier[j].fuel,1995,74(8):1216-1219.
|
| [27] | ibarrajv,molinerr,bonetaj.ft-irinvestigationoncharformationduringtheearlystagesofcoalpyrolysis[j].fuel,1994,73(6):918-924.
|
| [28] | painterpc,snyderrw,starsinicm,colemanmm,kuehndw,davisa.concerningtheapplicationofft-irtothestudyofcoal:acriticalassessmentofbandassignmentsandtheapplicationofspectralanalysisprograms[j].applspectrosc,1981,35(5):475-485.
|
| [29] | salemaaa,afzalmt,motasemif.istheresynergybetweencarbonaceousmaterialandbiomassduringconventionalpyrolysisatg-ftirapproach[j].janalapplpyrolysis,2014,105(1):217-226.
|
| [30] | solomonpr,carangelorm.ft-iranalysisofcoal[j].fuel,1988,67(7):949-959.
|
| [31] | russoc,stanzionef,tregrossia,ciajoloa.infraredspectroscopyofsomecarbon-basedmaterialsrelevantincombustion:qualitativeandquantitativeanalysisofhydrogen[j].carbon,2014,74:127-138.
|
Full-Text
|
|
Contact Us
service@oalib.com QQ:3279437679 
WhatsApp +8615387084133
|
|