|
|
Molbank 2008
One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazoleDOI: 10.3390/m577 Keywords: Microwave assisted synthesis, 1, 3-Dipolar cycloadditions, Benzyne intermediate, 1H-Phenanthro[9, 10-d][1, 2, 3]triazole, 1, 2, 3-Triazoles Abstract: In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.
|
