3D
supramolecular network with considerable volume pores was created via hydrogen
bond & C-H--π. By tightening of The metal-organic frameworks (MOF) namely [Ni(μ-pmb)2(H2O)2]n (pmb = 3,5-bis(4-pyridylmethylenoxyl)benzoate,
that have been synthesized by hydrothermal method. Complex 1 crystallizes in
triclinic P-1 space group and consists of 1D semi zigzag chain.
References
[1]
Barrer, R.M. (1982) Hydrothermal Chemistry of Zeolite. Academic Press, London.
[2]
Occelli, M.L. and Robson, H.C. (1989) Zeolite Synthesis. American Chemical Society, Washington DC. https://doi.org/10.1021/bk-1989-0398
[3]
Cheethman, A.K., Ferey, G. and Loiseau, T. (1999) Open-Framework Inorganic Materials. Angewandte Chemie International Edition, 38, 3268-3292. https://doi.org/10.1002/(SICI)1521-3773(19991115)38:22<3268::AID-ANIE3268>3.0.CO;2-U
[4]
Weller, M.T. and Dann, S.E. (1998) Hydrothermal Synthesis of Zeolites. Current Opinion in Solid State & Materials Science, 3, 137-143. https://doi.org/10.1016/S1359-0286(98)80078-8
[5]
Muller, A., Reuter, H. and Dillinger, S. (1995) Supramolecular Inorganic Chemistry: Small Guests in Small and Large Hosts. Angewandte Chemie International Edition, 34, 2311.
[6]
Hagrman, P.J., Hagrman, D. and Zubieta, J. (1999) Organic-Inorganic Hybrid Materials: From “Simple” Coordination Polymers to Organodiamine-Templated Molybdenum Oxides. Angewandte Chemie International Edition, 38, 2638-2684. https://doi.org/10.1002/(SICI)1521-3773(19990917)38:18<2638::AID-ANIE2638>3.0.CO;2-4
[7]
Rao, C.N.R. (2004) Metal Carboxylates with Open Architectures. Angewandte Chemie International Edition, 43, 1466-1496. https://doi.org/10.1002/anie.200300588
[8]
Seo, J.S., Wang, D., Lee, H., Jun, I., Oh, J., Jeon, Y.J. and Kim, K. (2000) A Homochiral Metal-Organic Porous Material for Enantioselective Separation and Catalysis. Nature (London), 404, 982-986. https://doi.org/10.1038/35010088
[9]
Lin, W., Evans, O.R., Xiong, R.G. and Wang, Z.J. (1998) Supramolecular Engineering of Chiral and Acentric 2D Networks. Synthesis, Structures, and Second-Order Nonlinear Optical Properties of Bis(nicotinato)zinc and Bis{3-[2-(4-pyridyl)ethenyl]benzoato}cadmium. Journal of the American Chemical Society, 120, 13272-13273. https://doi.org/10.1021/ja983415h
[10]
Pang, J.E., Marcotte, J.P., Seward, C., Brown, R.S. and Wang, S.N. (2001) A Blue Luminescent Star-Shaped ZnII Complex that Can Detect Benzene. Angewandte Chemie International Edition, 40, 4042-4045. https://doi.org/10.1002/1521-3773(20011105)40:21<4042::AID-ANIE4042>3.0.CO;2-0
[11]
Inoue, K., Imai, H., Ghalsasi, P.S., Kikuchi, K., Ohba, M., Okawa, H. and Yakhmi, J.V. (2001) A Three-Dimensional Ferrimagnet with a High Magnetic Transition Temperature (TC) of 53 K Based on a Chiral Molecule. Angewandte Chemie International Edition, 40, 4242-4245. https://doi.org/10.1002/1521-3773(20011119)40:22<4242::AID-ANIE4242>3.0.CO;2-H
[12]
Cave, D.J., Gascon, M., Bond, A.D., Teat, S.J. and Wood, P.T. (2002) Layered Metal Organosulfides: Hydrothermal Synthesis, Structure and Magnetic Behaviour of the Spin-Canted Magnet Co(1,2-(O2C)(S)C6H4). Chemical Communications, 1050-1051. https://doi.org/10.1039/b111339a
[13]
Wang, X., Qin, C., Wang, E., Li, Y., Hao, N., Hu, C. and Xu, L. (2004) Syntheses, Structures, and Photoluminescence of a Novel Class of d10 Metal Complexes Constructed from Pyridine-3,4-dicarboxylic Acid with Different Coordination Architectures. Inorganic Chemistry, 43, 1850-1856. https://doi.org/10.1021/ic035151s
[14]
Dong, Y.B., Cheng, J.Y., Huang, R.Q., Smith, M.D. and Zur Loye, Y.B. (2003) Self-Assembly of Coordination Polymers from AgX (X = SbF6-, PF6-, and CF3SO3-) and Oxadiazole-Containing Ligands. Inorganic Chemistry, 42, 5699.
[15]
Galan-Mascaros, J.R. and Dunbar, K.R. (2003) A Self-Assembled 2D Molecule-Based Magnet: The Honeycomb Layered Material {Co3Cl4(H2O)2[Co(Hbbiz) 3]2}. Angewandte Chemie International Edition, 42, 2289-2293. https://doi.org/10.1002/anie.200250152
[16]
Cui, Y., Lee, S.J. and Lin, W.J. (2003) Interlocked Chiral Nanotubes Assembled from Quintuple Helices. Journal of the American Chemical Society, 125, 6014-6015. https://doi.org/10.1021/ja029926s
[17]
Horikoshi, R., Mochida, T. and Moriyama, H. (2002) Synthesis and Characterization of Redox-Active Coordination Polymers Generated from Ferrocene-Containing Bridging Ligands. Inorganic Chemistry, 41, 3017-3024. https://doi.org/10.1021/ic011176k
[18]
Chen, L.C., Su, C.Y., Cai, Y.P., Zhang, H.X., Xu, A.W., Kang, B.S. and Zur, H.C. (2003) Multidimensional Frameworks Assembled from Silver(I) Coordination Polymers Containing Flexible Bis(thioquinolyl) Ligands: Role of the Intra- and Intermolecular Aromatic Stacking Interactions. Inorganic Chemistry, 42, 3738-3750. https://doi.org/10.1021/ic0341035
[19]
Bu, X.H., Hou, W.F., Du, M., Chen, W.R. and Zhang, H. (2002) Varying the Frameworks of Novel Silver(I) Coordination Polymers with Thioethers by Altering the Backbone or Terminal Groups of Ligands. Crystal Growth & Design, 2, 303-307. https://doi.org/10.1021/cg025510e
[20]
Khlobystor, A.N., Blake, A.J., Champness, N.R., Lemenovskii, D.A., Majouga, A.G., Zyk, N.V. and Schröder, M. (2001) Supramolecular Design of One-Dimensional Coordination Polymers Based on Silver(I) Complexes of Aromatic Nitrogen-Donor Ligands. Coordination Chemistry Reviews, 222, 155-192. https://doi.org/10.1016/S0010-8545(01)00370-8
[21]
Hirsch, K.A., Wilson, S.R. and Moore, J.S. (1997) Coordination Networks of 3,3’-Dicyanodiphenylacetylene and Silver(I) Salts: Structural Diversity through Changes in Ligand Conformation and Counterion. Inorganic Chemistry, 36, 2960-2968. https://doi.org/10.1021/ic970150j
[22]
Masood, M.A., Enemark, E.J. and Stack, T.D.P. (1998) Ligand Self-Recognition in the Self-Assembly of a [{Cu(L)}2]2+ Complex: The Role of Chirality. Angewandte Chemie International Edition, 37, 928-932. https://doi.org/10.1002/(SICI)1521-3773(19980420)37:7<928::AID-ANIE928>3.0.CO;2-T
[23]
Hartshorn, C.M. and Steel, P.J. (1997) Self-Assembly and X-Ray Structure of a Ten-Component, Three-Dimensional Metallosupramolecular Cage. Chemical Communications, No. 6, 541. https://doi.org/10.1039/a608081b
[24]
Hennigar, T.L., MacQyarrie, D.C., Losier, P., Rogers, R.D. and Zaworotko, M.J. (1997) Supramolecular Isomerism in Coordination Polymers: Conformational Freedom of Ligands in [Co(NO3)2(1,2-bis(4-pyridyl)ethane)1.5]n. Angewandte Chemie International Edition, 36972.
[25]
Wang, Q.M., Guo, G.C. and Mak, T.C.W. (1999) A Coordination Polymer Based on Twofold Interpenetrating Three-Dimensional Four-Connected Nets of 42638 Topology, [CuSCN(bpa)] [bpa = 1,2-bis(4-pyridyl)ethane]. Chemical Communications, No. 18, 1849-1850. https://doi.org/10.1039/a905085j
[26]
Kondo, M., Shimamura, M., Noro, S., Kimura, Y., Uemura, K. and Kitagawa, S. (2000) Synthesis and Structures of Coordination Polymers with 4,4'-dipyridyldisulfide. Journal of Solid State Chemistry, 162, 113.
[27]
Tabellion, F.M., Seidel, S.R., Arif, A.M. and Stang, P.J. (2001) Discrete Supramolecular Architecture vs Crystal Engineering: The Rational Design of a Platinum-Based Bimetallic Assembly with a Chairlike Structure and Its Infinite, Copper Analogue. Journal of the American Chemical Society, 123, 7740-7741. https://doi.org/10.1021/ja015784a
[28]
Wang, R., Han, L., Jiang, F., Zhou, Y., Yuan, D. and Hong, M. (2005) Syntheses and Crystal Structures of Copper(II) Coordination Polymers Comprising Discrete Helical Chains. Crystal Growth & Design, 5, 251-256. https://doi.org/10.1021/cg034237t
[29]
Aakeröy, C.B. and Seddon, K.R. (1993) The Hydrogen Bond and Crystal Engineering. Chemical Society Reviews, 22, 397-407. https://doi.org/10.1039/CS9932200397
[30]
Jeffery, G.A. (1997) Introduction to Hydrogen Bonding. Wiley, Chichester.
[31]
Atwood, J.L., Barbour, L.J. and Jerga, A. (2004) Angewandte Chemie International Edition, 432948.
[32]
Sada, K., Tanaka, K.T., Tanaka, A., Epergyes, A., Nagahama, S., Matsumoto, A. and Miyata, M. (2004) Organic Layered Crystals with Adjustable Interlayer Distances of 1-Naphthylmethylammonium n-Alkanoates and Isomerism of Hydrogen-Bond Networks by Steric Dimension. Journal of the American Chemical Society, 126, 1764-1771. https://doi.org/10.1021/ja038379n
[33]
Higashi, T. (1995) Program for Absorption Correction. Rigaku Corporation, Tokyo.
[34]
(1997) SHELXTL, Version 5.1. Siemens Industrial Automation, Inc., Tokyo.
[35]
Fifield, F.W. and Kealy, D. (2000) Principles and Practice of Analytical Chemistry. 5th Edition, Blackwell Science, Oxford, 378-393.
