|
100t EAF-LF-VD-CC流程中H13模具钢夹杂物的演变行为
|
Abstract:
本文针对100t EAF→LF精炼→VD处理→连铸流程生产的H13模具钢为研究对象,应用金相显微镜和扫描电镜分别对生产各环节钢中夹杂物的分布、尺寸、数量、微观形貌及成分进行检验分析。结果表明,钢中夹杂物由数量多、颗粒大逐渐转变为数量少、颗粒小;夹杂物面积百分比呈下降趋势;在夹杂物尺寸方面,呈现先由小变大再变小;在夹杂物的成分方面,开始由大量的单颗粒的Al2O3、团簇状Al2O3组成,随着工艺的进行成分以复合类的夹杂物为主,典型代表有CaO-Al2O3-MgO-SiO2、MgO-CaO-Al2O3、Al2O3-CaO-MgO-SiO2等夹杂。
In this paper, the H13 die steel produced by 100t EAF→LF→VD→continuous casting process is studied. The distribution, size, quantity and microstructure of inclusions in steel are produced by metallographic microscope and scanning electron microscope. After inspection and analysis, it can be seen that the distribution of inclusions is changed from a large amount to a small amount, and the particles are small; the percentage of inclusions is decreasing; in terms of inclusion size, and it is changed from small to large, then small; in terms of the composition of inclusions, it begins with a large number of single-particle Al2O3 and cluster-like Al2O3. As the process proceeds, the compo-sition is mainly composed of composite inclusions, typically CaO-Al2O3-MgO-SiO2, MgO-CaO-Al2O3, and Al2O3-CaO-MgO-SiO2.
[1] | 崔崑. 国内外模具用钢发展概况[J]. 金属热处理, 2007, 32(1): 1-4. |
[2] | 庞永刚, 侯明山, 胡建成, 等. 40t EBT-LF-VD-铸锭工艺冶炼模具钢H13旳洁净度分析[J]. 特殊钢, 2013, 34(5): 61-63. |
[3] | 刘少友, 何建武. 热作模具钢H13圆棒生产实践[J]. 武钢技术, 2015, 53(6): 24-27. |
[4] | Ma, W.J., Bao, Y.P., Wang, M., et al. (2014) Ef-fect of Mg and Ca Treatment on Behavior and Particle Size of Inclusions in Bearing Steels. ISIJ International, 54, 536-542. https://doi.org/10.2355/isijinternational.54.536 |
[5] | Dogan, N., Longbottom, R.J., Reid, M.H., et al. (2014) Morphology and Composition Changes of Spinel MgAl2O4 Inclusions in Steel. Ironmaking & Steelmaking, 42, 185-193. https://doi.org/10.1179/1743281214Y.0000000219 |
[6] | 王淑华, 丛玉伟, 李雪峰. 高品质H13模具钢质量研究与分析[J]. 河南冶金, 2010, 18(2): 29-30. |
[7] | 阳燕, 刘建华, 包燕平等. 热作模具钢 H13 的非金属夹杂物研究[J]. 钢铁, 2011, 46(9): 45-49. |
[8] | 王亮亮. 镁对H13热作模具钢夹杂物及性能影响的研究[D]: [博士学位论文]. 北京: 北京科技大学, 2014. |
[9] | 刘建华, 阳燕, 庄昌凌, 等. H13模铸钢锭中夹杂物的分布解剖[J]. 北京科技大学学报, 2011, 33(31): 179-183. |