OALib Journal期刊
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用ni(oh)2浆化氢还原法制备纳米金属镍粉的反应机制
Keywords: ni(oh)2,氢气还原,纳米镍粉,反应机制
Abstract:
?用ni(oh)2浆液水热氢还原法制备了纳米金属镍粉,通过对不同反应阶段样品性质的分析,研究了反应的机制。结果表明,在酸性条件下,通过复盐离解出的镍离子在溶液中与氢发生反应;在碱性条件下,ni(oh)2固体颗粒直接与活性氢发生反应。
References
[1] | 1n.brown,z.j.zhou,testsfordevelopinggaspiperesins,plastic,rubberandcomposites,34,289(2005)
|
[2] | 2y.l.huang,n.brown,dependenceofslowcrackgrowthinpolythyleneonbutylbranchdensity:morphologyandtheory,j.polym.sci.,partb:polym.phys.,29,129(1991)
|
[3] | 17r.seguela,criticalreviewofthemoleculartopologyofsemicrystallinepolymers:theoriginandassessmentofin-tercrystallinetiemoleculesandchainentanglements.j.polym.sci.,partb:polym.phys.,43,1729(2005)
|
[4] | 18b.wunderlich,macromolecularphysics,vol.3,crystalmelting,academicpress,newyork,1980.
|
[5] | 19d.massiot,f.fayon,m.capron,l.king,s.l.calvé,b.alouso,j.o.durand,b.bujoli,z.gan,g.hoatson,mod-ellingone-andtwo-dimensionalsolid-statenmrspectra,magn.reson.chem.,40,70(2001)
|
[6] | 20a.buda,d.demco,m.bertmer,b.blümich,b.reining,h.keul,h.hscker,domainsizesinheterogeneouspoly-mersbyspindiffusionusingsingle-quantumanddouble-quantumdipolarfilters.solidstatenucl.magn.reson.,24,39(2003)
|
[7] | 21a.m.e.baker,a.h.windle,evidenceforapartiallyor-deredcomponentinpolyethylenefromwide-anglex-raydiffraction,polymer,42,667(2002)
|
[8] | 22l.mandelkern,thestructureofcrystallinepolymers,acc.chem.res.,3,347(1992)
|
[9] | 23r.r.eckman,p.m.henrichs,a.t.peacock,studyofpoly-ethylenebysolidstatenmrrelaxationandspindiffusion.macromolecules,30,2474(1997)
|
[10] | 24s.gautam,s.balijepalli,g.c.rutledge,molecularsimula-tionsoftheinterlamellarphaseinpolymers:effectofchaintilt.macromolecules,33,9136(2000)
|
[11] | 31s.kavesh,j.m.schultz,lamellarandinterlamellarstruc-tureinmelt-crystallizedpolyethylene.i.degreeofcrys-tallinity,atomicpositions,particlesize,andlatticedisor-derofthefirstandsecondkinds.j.polym.sci.,parta:polym.chem.,8,243(1970)
|
[12] | 32p.j.deslanriers,m.p.mcdaniel,d.c.rohlfing,r.k.krishnaswamy,s.j.secora,e.a.benham,p.l.maeger,a.r.wolfe,a.m.sukhadia,b.b.beaulieu,acomparativestudyofmultimodalvs.bimodalpoly-ethylenepiperesionsforpe100applications.polym.eng.sci.,45(9),1203(2005)
|
[13] | 3x.lu,n.brown,therelationshipoftheinitiationstagetotherateofslowcrackgrowthinlinearpolyethylene,j.mater.sci.,21,2423(1986)
|
[14] | 4l.l.b(?)hm,h.f.enderle,m.fleissner,high-densitypoly-ethylenepiperesins,adv.mater.,4,234(1992)
|
[15] | 5y.l.huang,n.brown,thedependenceofbutyldensityonslowcrackgrowthinpolyethylene:kinetics,j.polym.sci.,partb:polym.phys.,28,2007(1990)
|
[16] | 6x.lu,q.wang,n.brown,slowfractureinahomopoly-merandcopolymerofpolyethylene,j.mater.sci.,23,643(1988)
|
[17] | 7l.hubert,l.david,r.séguéla,g.vigier,c.corfias-zuccalli,y.germain,physicalandmechanicalpropertiesofpolyethyleneforpipesinrelationtomoleculararchitec-ture.i.microstructureandcrystallisationkenetics.poly-mer,42,8425(2001)
|
[18] | 8l.hubert,l.david,r.séguéla,g.vigier,c.corfias-zuccalli,y.germain,physicalandmechanicalpropertiesofpolyethyleneforpipesinrelationtomoleculararchitec-ture.ⅱ.short-termcreepofisotropicanddrawnmateri-als,j.appl.polym.sci.,84,2308(2002)
|
[19] | 9gerogec.oppenlander,structureandpropertiesofcrys-tallinepolymers,sceience,159,1311(1968)
|
[20] | 10a.d.channell,e.q.clutton,theeffectsofshortchainbranchingandmolecularweightontheimpactfracturetoughnessofpolyethylene,polymer,33,4108(1992)
|
[21] | 11x.lu,r.qian,n.brown,theeffectofcrystallinityonfractureandyieldingofpolyethylenes,polymer,36,4239(1995)
|
[22] | 12m.fleissner,diespezifischebruchenergieyonpolyethyleninabh(?)ngigkeityonstrukturellenparametern,angew.makromol.chem.,105,167(1982)
|
[23] | 13y.f.men,j.rieger,h.f.enderle,d.lilge,themobilityoftheamorphousphaseinpolyethyleneasadeterminingfac-torforslowcrackgrowth.theeuropeanphysicaljournale,15,421(2004)
|
[24] | 14hanwei,zouguangtian,tengfengen,wangyum-ing,v.e.panin,a.i.slosman,plasticdeformationandfractureofpartiallycrystallinepolyethylene,chin.j.mater.res.,14(5),548(2000)(韩炜,邹广田,膝凤恩,王煜明,v.e.panin,a.i.slosman,半晶聚乙烯介观结构变化的x射线研究,材料研究学报,14(5),548(2000))
|
[25] | 15b.bliimich,nmrimagingofmaterials,oxforduniver-sitypress,oxford,2000
|
[26] | 16a.ahvenainen,k.sarantila,h.andtsjoe,j.takakarhu,a.palmroos,multi-stageprocessforproducingpoly-ethylene,wopatent,wo9212182(1992)
|
[27] | 25d.a.ivanov,t.pop,d.y.yoon,a.m.jonas,directobser-vationofcrystal-amorphousinterphaseinlamellarsemi-crystallinepoly(ethyleneterephthalate),macromolecules,35,9813(2002)
|
[28] | 26k.bergmann,studyofthemolecularmotionsofpoly-ethylenebyline-shapeanalysisofbroad-lineprotonnmrspectra,j.polym.sci.,partb:polym.phys.,16,1611(1978)
|
[29] | 27l.mandelkern,therelationbetweenstructureandprop-ertiesofcrystallinepolymers.polym.j.,17,337(1985)
|
[30] | 28m.hedenqvist,a.angelstok,l.edsberg,p.t.larssonandu.w.gedde,diffusionofsmall-moleculepenetrantsinpolyethylene:freevolumeandmorphology.polymer,37,2887(1996)
|
[31] | 29b.neway,m.s.hedenqvist,u.w.gedde,effectofthermalhistoryonfreevolumeandtransportpropertiesofhighmolarmasspolyethylene.polymer,44,4003(2003)
|
[32] | 30d.demco,a.johansson,protonspindiffusionforspa-tialheterogeneityandmorphologyinvestigationsofpoly-mers,j.tegenfeldt,solidstatenucl.magn.reson.,4,13(1995)
|
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