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OALib Journal期刊
ISSN: 2333-9721
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不使用保护气氛和还原剂超声制备纳米钯颗粒
Abstract:
？在存在微量聚乙烯吡咯烷酮(pvp)、不用气氛保护和还原剂的条件下超声还原氯化钯水溶液,合成出单分散纳米金属钯粒子,用tem、hrtem、ft-ir、xrd等技术进行了表征.tem、hrtem观察表明纳米金属钯粒子表现出单分散性,为柱状晶体;纳米钯粒子在溶液中的稳定分散存在主要与ftir揭示的pvp羰基基团与钯原子存在一定的配位吸附作用和pvp的长链空间位阻效应有关.
| [1] | 1g.p.sabol,g.r.kilp,m.g.balfour,e.roberts,develop-mentofacladdingalloyforhighburnup,in:zirconiuminthenuclearindustry,eighthinternationalsymposium,editedbyl.f.p.vanswamandc.m.eucken(america,astmspec.tech.publ.1023,1989)p.227
|
| [2] | 2r.j.comstock,g.schoenberger,g.p.sabol,influenceofprocessingvariablesandalloychemistryonthecorrosionbehaviorofzirlonuclearfuelcladding,in:zirconiuminthenuclearindustry,eleventhinternationalsymposium,editedbye.r.bradleyande.r.sabol(america,astmspec.tech.publ.1295,1996)p.710
|
| [3] | 3a.v.nikulina,v.a.markelov,m.m.peregud,zirconiumalloye635asamaterialforfuelrodcladdingandothercomponentsofvverandrbmkcores,in:zirconiuminthenuclearindustry,eleventhinternationalsymposium,editedbye.r.bradleyande.r.sabol(america,astmspec.tech.publ.1295,1996)p.785
|
| [4] | 4j.y.park,b.k.choi,s.j.yoo,y.h.jeong,corrosionbe-haviorandoxidepropertiesofzr-1.1wt%nb-0.05wt%cualloy,journalofnuclearmaterials,359(1),59(2006)
|
| [5] | 13t.arima,k.miyata,y.inagaki,k.idemitsu,oxidationpropertiesofzr-nballoysat500-600℃underlowoxygenpotentials,corrosionscience,47,435(2005)
|
| [6] | 14lizhongkui,liujianzhang,zhoulian,licong,zhangjianjun,studyonmicrostructureofoxidefilmfornewzirconiumalloys,raremetalmaterialsandengi-neering,31(4),261(2002)(李中奎，刘建章，周廉，李聪，张建军，新锆合金氧化膜微观组织结构的研究，稀有金属材料与工程，31(4)，261(2002))
|
| [7] | 5a.t.motta,a.yilmazbayhan,m.j.g.silva,r.j.comstock,g.s.was,j.t.busby,e.gartner,q.j.peng,y.h.jeong,j.y.park,zirconiumalloysforsupercriticalwaterreac-torapplications:challengesandpossibilities,journalofnuclearmaterials,371,61(2005)
|
| [8] | 6a.grandjean,y.serruys,metalandoxygenmobilitiesdur-ingzircaloy-4oxidationathightemperature,journalofnuclearmaterials,273(1),111(1999)
|
| [9] | 7m.oskarsson,e.ahlberg,u.andersson,k.pettersson,characterisationofpre-transitionoxidesonzircaloys,journalofnuclearmaterials,297(1),77(2001)
|
| [10] | 8l.gosmain,c.valot,d.ciosmak,o.sicardy,studyofstresseffectsintheoxidationofzircaloy-4,solidstateionics,141,633(2001)
|
| [11] | 9zhaowenjin,miaozhi,jianghongman,yuxi-aowei,liweijun,licong,zhoubangxin,corrosionbehaviorofzr-sn-nballoy,journalofchinesesocietyforcorrosionandprotection,22(2),124(2002)(赵文金，苗志，蒋宏曼，于晓卫，李卫军，李聪，周邦新，zr-sn-nb合金的腐蚀行为研究，中国腐蚀与防护学报，22(2)，124(2002))
|
| [12] | 10zhoubangxin,liqiang,huangqiang,miaozhi,zhaowenjin,licong,theeffectofwaterchemistryoncorrosionresistanceofzirconiumalloys,nuclearpowerengineering,21(5),439(2000)(周邦新，李强，黄强，苗志，赵文金，李聪，水化学对锆合金耐腐蚀性能影响的研究，核动力工程，21(5)，439(2000))
|
| [13] | 11zhoubangxin,liqiang,yaomeiyi,liuwenqing,thegrainsmorphologyofoxidefilmsforzircolay-4,raremetalmaterialsandengineering,32(6),417(2003)(周邦新，李强，姚美意，刘文庆，锆-4合金氧化膜中晶粒形貌观察，稀有金属材料与工程，32(6)，417(2003))
|
| [14] | 12liuwenqing,chenwenjue,liqiang,zhoubangxin,yaomeiyi,effectofwaterchemistryonoxidemorph-plogiesofzircaloy-4,nuclearpowerengineering,25(6),517(2004)(刘文庆，陈文觉，李强，周邦新，姚美意，水化学对zr-4合金氧化膜形貌的影响，核动力工程，25(6)，517(2004))
|
| [15] | 15y.h.jeong,k.o.lee,h.g.kim,correlationbetweenmi-crostructureandcorrosionbehaviorofzr-nbbinaryalloy,journalofnuclearmaterials,302,9(2002)
|
| [16] | 16y.h.jeong,h.g.kim,t.h.kim,effectofβphase,pre-cipitateandnb-concentrationinmatrixoncorrosionandoxidecharacteristicsofzr-xnballoys,journalofnuclearmaterials,317,1(2003)
|
| [17] | 17a.j.g.maroto,r.bordoni,m.villegas,a.m.olmedo,m.a.blesa,a.iglesias,p.koenig,growthandcharacter-izationofoxidelayersonzirconiumalloys,journalofnu-clearmaterials,229,79(1996)
|
| [18] | 18p.bouvier,j.godlewski,g.lucazeau,aramanstudyofthenanocrystallitesizeeffectonthepressure-temperaturephasediagramofzirconiagrownbyzirconium-basedalloysoxidation,journalofnuclearmaterials,300,118(2002)
|
| [19] | 19y.h.jeong,j.h.baek,s.j.kim,h.g.kim,h.ruhmann,corrosioncharacteristicsandoxidemicrostructuresofzircaloy-4inaqueousalkalihydroxidesolution,journalofnuclearmaterials,270,322(1999)
|
| [20] | 20n.pétigny,p.barberis,c.lemaignan,ch.valot,m.lallemant,insituxrdanalysisoftheoxidelay-ersformedbyoxidationat743konzircaloy-4andzr-1nbo,journalofnuclearmaterials,280,318(2000)
|
| [21] | 21a.yilmazbayhan,e.breval,a.t.motta,r.j.comstock,transmissionelectronmicroscopyexaminationofoxidelayersformedonzralloys,journalofnuclearmaterials,349,265(2006)
|
| [22] | 22p.barberis,t.merle-méjean,p.quintard,onramanspec-troscopyofzirconiumoxidefilms,journalofnuclearma-terials,246(3),232(1997)
|
| [23] | 23p.barbéris,g.corolleur-thomas,r.guinebretière,t.merle-mejean,a.mirgorodsky,p.quintard,ramanspectraoftetragonalzirconia:powdertozircaloyoxidefrequencyshift,journalofnuclearmaterials,288(3),241(2001)
|
| [24] | 24j.godlewski,j.p.gross,m.lambertin,j.f.wadier,h.weidinger,ramanspectroscopystudyofthetetragonaltomonoclinictransitioninoxidescalesanddeterminationofoveralloxygendiffusionbynuclearmicroanalysisofo18,in:zirconiuminthenuclearindustry,ninthinternationalsymposium,editedbyc.m.euckenanda.m.grade(america,astmspec.tech.publ.1132,1991)p.416
|
| [25] | 25zhanghaixia,lizhongkui,d.fruchart,zhangtingjie,zhangjianjun,zhoujun,zhoulian,crys-talstructureanalysisofoxidefilmofnewzirconiumalloy,raremetalmaterialsandengineering,35(12),1908(2006)(章海霞，李中奎，d．fruchart，张廷杰，张建军，周军，周廉，新锆合金氧化膜的晶体结构分析，稀有金属材料与工程，35(12)，1908(2006))
|
| [26] | 26t.arima,k.miyata,y.inagaki,k.idemistu,oxidationpropertiesofzr-nballoysat500-600℃underlowoxygenpotentials,corrosionscience,47,435(2005)
|
| [27] | 27p.barberis,zirconiapowdersandzircaloyoxidefilms:tetragonalphaseevolutionduring400℃autoclavetests,journalofnuclearmaterials,226,34(1995)
|
| [28] | 28j.godlewski,howthetetragonalzirconiaisstabilizedintheoxidescalethatisformedonazirconiumalloycor-rodedat400℃insteam,in:zirconiuminthenu-clearindustry-thenthinternationalsymposium,editedbya.m.gardeande.r.bradley(america,astmspec.tech.publ.1245,1993)p.663x
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