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单体/交联剂比例对聚丙烯酰胺凝胶法制备纳米beo粉体的影响

Keywords: 纳米beo,聚丙烯酰胺凝胶法,单体--交联剂比例,纳米粉体

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Abstract:

?研究了单体/交联剂比例对聚丙烯酰胺凝胶法制备纳米粉体beo过程和特征的影响。结果表明:??三维结构的高分子网络结构将盐细化,使其热分解温度明显降低。当单体和交联剂的质量比为6:1时,热分解温度下降幅度最大,约为177℃;所制备的粉体的平均颗粒尺寸也最小,约为16nm,粒度分布范围较窄且团聚少。当单体和交联剂的质量比偏离6:1时,热分解温度下降幅度减少,所制备的粉体的颗粒尺寸增加。

References

[1]  nimeng,leungmichaelk.h..leungdennisy.c..technologydevelopmentinnano-sizedphotocatalystpowderpreparationtechnologies.powdermetallurgytechnology,2006,24:379-383
[2]  igordjerdj,denisar?on,zvonkojagli?i?,markusniederberger.nonaqueoussynthesisofmetaloxidenanoparticles:shortreviewanddopedtitaniumdioxideascasestudyforthepreparationoftransitionmetal-dopedoxidenanoparticles.journalofsolidstatechemistry,2008,181:1571-1581
[3]  douya.,odierp..thepolyacrylamidegel:anovelroutetoceramicandglassyoxidepowders.materialsresearchbulletin,1989,24:1119-1126
[4]  shaozhongbao,liguo-rong.prepararionofnanometer-sizedzincoxidepowdersbypolyacrylamidegelmethod.chinesejournalofmaterialsresearch,2001,15:681-685
[5]  chuanyipan,xuehuili,furongwang,lefuwang.synthesisofbismuthoxidenanoparticlesbythepolyacrylamidegelroute.ceramicsinternational,2008,34:439-441
[6]  (潘祖仁,高分子化学(北京,化学工业出版社,2006)p.78-80
[7]  14fangdaobin,guoruiwei,harunhua,polymersofacrylamide,(beijing,chemicalindustrypress,2006)p.143-18
[8]  李金峰,孙以实,阮竹,丙烯酰胺与n.n’-亚甲基双丙烯酰胺的共聚反应研究.高分子学报,1990,5:593-599
[9]  倪萌,leungmichaelk.h.,leungdennisy.c..光催化剂纳米粉体的制备技术.粉末冶金技术,2006,24:379-383
[10]  g.c.c.costa,r.muccillo.synthesisofscandia-stabilizedzirconiananoparticlesbythepolyacrylamidetechnique.solidstateionics,2008,179:1219-1222
[11]  andrédouy.polyacrylamidegel:anefficienttoolforeasysynthesisofmulticomponentoxideprecursorsofceramicsandglasses.internationaljournalofinorganicmaterials,2001,3:699-707
[12]  邵忠宝,李国荣.高分子网络凝胶法制备纳米zno粉料.材料研究学报,2001,15:681-685
[13]  h.wang,l.gao,weiqunli,qiangli.preparationofnanoscaleα-al2o3bythepolyacrylamidegelmethod.nanostructuredmaterials,1999,11:1263-1267
[14]  m.tahmasebpour,a.a.babaluo,s.shafiei,e.pipelzadeh.studiesonthesynthesisofα-al2o3nanopowdersbythepolyacrylamidegelmethod.powdertechnology,2009,191:91-97
[15]  m.tahmasebpour,a.a.babaluo,m.k.razaviaghjeh.synthesisofzirconiananopowdersfromvariouszirconiumsaltsviapolyacrylamidegelmethod.journaloftheeuropeanceramicsociety,2008,28:773-778
[16]  ningliu,yupengyuan,p.majewski,f.aldinger.synthesisofla0.85sr0.15ga0.85mg0.15o2.85materialsforsofcapplicationsbyacrylamidepolymerization.materialsresearchbulletin,2006,41:461-468
[17]  a.tarancón,g.dezanneau,j.arbiol,f.peiro.j.r.morante.synthesisofnanocrystallinematerialsforsofcapplicationsbyacrylamidepolymerization.journalofpowersources,2003,118:256-264
[18]  13panzuren,polymerchemistry,(beijing,chemicalindustrypress,2006)p.78-8
[19]  (方道斌,郭睿威,哈润华,丙烯酰胺聚合物,(北京,化学工业出版社,2006)p.143-181
[20]  dollimored.,konieczayj.l..thethermaldecompositionofberylliumoxalateandrelatedmaterials.thermochimicaacta,1998,318:155-163
[21]  lijinfeng,sunyishi,runzhu,oncopolymerizationofacrylamidewithn.n’–methylenebisacylamide.actapolymericasinica,1990,5:593-599

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