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OALib Journal期刊
ISSN: 2333-9721
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铝阳极氧化膜纳米孔阵列的微细结构
Keywords: 无机非金属材料,多孔阳极氧化铝膜(aao
Abstract:
？用电化学阳极氧化法制备了纳米多孔铝阳极氧化膜(aao模板).采用原子力显微镜(afm)测试aao膜,研究了纳米孔阵列的形成机制.结果表明,在aao膜的表面,除存在六方形的纳米孔阵列外,在孔端还存在六个微小的隆起,相邻的隆起之间彼此相连,看上去酷似一朵盛开的梅花,花的中心就是六方形纳米孔.二维afm图像显示,以往用扫描电镜表征的纳米孔阵列,实际上是一幅排列整齐、并呈周期性变化的梅花阵列图案.膜背面阻挡层的afm二维图像表明,膜胞呈六方形,且排列高度有序.膜胞密度为4.3？109/cm2,与孔密度基本一致.阻挡层的三维照片显示,膜胞的底部存在半球状突起,也呈现出规整的阵列图案.
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