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涂料工业  2013 

涂料中16种多环芳烃的气相色谱-质谱法研究

Keywords: 多环芳烃,气相色谱-质谱,前处理,内标法

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Abstract:

?对涂料中16种多环芳烃含量检测的前处理方法做了系统的优化。在优化条件下采用气相色谱-质谱并运用内标法,建立了涂料中多环芳烃物质的定性定量分析方法。该方法的线性相关系数均大于0.999,显示出较好的线性关系,检出限在0.001~0.02mg/kg之间。方法回收率为77.87%~116.84%,精密度(n=7)为2.36%~8.63%。对各种类型的市售涂料进行实际样品的检测,结果令人满意。

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