OALib Journal期刊
ISSN: 2333-9721
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涂料中16种多环芳烃的气相色谱-质谱法研究
Keywords: 多环芳烃,气相色谱-质谱,前处理,内标法
Abstract:
?对涂料中16种多环芳烃含量检测的前处理方法做了系统的优化。在优化条件下采用气相色谱-质谱并运用内标法,建立了涂料中多环芳烃物质的定性定量分析方法。该方法的线性相关系数均大于0.999,显示出较好的线性关系,检出限在0.001~0.02mg/kg之间。方法回收率为77.87%~116.84%,精密度(n=7)为2.36%~8.63%。对各种类型的市售涂料进行实际样品的检测,结果令人满意。
References
[1] | wangah,zhangj,dingyc,etal.quantitativedeterminationof16polycyclicaromatichydrocarbonsinsoilsamplesusingsolid-phasemicroextraction[j].journalofseparationscience,2009(32):3951-3957.
|
[2] | 王成云,张伟亚,杨左军,等.高效液相色谱法测定有机硅涂料中多环芳烃[j].涂料工业,2007,37(8),46-49.
|
[3] | 卫碧文,于文佳,郑翊,等.gc-ms测定纺织品中多环芳烃[j].印染,2010(5):38-40.
|
[4] | johnsonys.determinationofpolycyclicaromatichydrocarbonsinedibleseafoodbyquechers-basedextractionandgaschromatography-tandemmassspectrometry[j].journaloffoodscience,2012,77(7):131-137.
|
[5] | fabbrid,adamianoa,torric.gc-msdeterminationofpolycyclicaromatichydrocarbonsevolvedfrompyrolysisofbiomass[j].analyticalandbioanalyticalchemistry,2010,397(1):309-317.
|
[6] | 陈皓,刘颖,刘海玲,等.超高效液相色谱法检测土壤中的多环芳烃[j].色谱,2008,26(6):769-771.
|
[7] | saravanabhavang,helfertya,hodsonpv,etal.amulti-dimensionalhighperformanceliquidchromatographicmethodforfingerprintingpolycyclicaromatichydrocarbonsandtheiralkyl-homologsintheheavygasoilfractionofalaskannorthslopecrude[j].journalofchromatographya,2007,1156(1-2):124-133.
|
[8] | 毛明英,刘守琼,宋磊,等.塑料食品包装制品中多环芳烃的分析及检测[j].包装工程,2009,30(1):43-45.
|
[9] | 王成云,唐莉纯,樊秀荣.涂料中多环芳烃的测定[j].上海涂料,2007,45:34-39.
|
[10] | menzieca,potockibb,santodonatoj.exposuretocarcinogenicpahsintheenvironment[j].environmentalscienceandtechnology,1992(26):1278-1284.
|
[11] | ishizakia,saitok,haniokan,etal.determinationofpolycyclicaromatichydrocarbonsinfoodsamplesbyautomatedon-linein-tubesolid-phasemicroextractioncoupledwithhigh-performanceliquidchromatography-fluorescencedetection[j].journalofchromatographya,2010,1217(35):5555-5563.
|
[12] | itohn,numatam,aovagiy,etal.comparisonoflow-levelpolycyclicaromatichydrocarbonsinsedimentrevealedbysoxhletextraction,microwave-assistedextraction,andpressurizedliquidextraction[j].analyticachimicaacta,2008,612(1):44-52.
|
[13] | 王洋,王彩虹.水泵橡胶密封件中多环芳烃的研究[j].农业机械学报,2009,40(12):113-118.
|
[14] | dongcd,chencf,chencw.determinationofpolycyclicaromatichydrocarbonsinindustrialharborsedimentsbygc-ms[j].internationaljournalofenvironmentalresearchandpublichealth,2012(9):2175-2188.
|
[15] | 李核,李攻科,陈洪伟.微波辅助萃取,气相色谱-质谱法测定大气可吸入颗粒物中痕量多环芳烃[j].分析化学,2002,30(9):1058-1062.
|
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