OALib Journal期刊
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麻疯树脱油种仁的总生物碱:提取及酸性染料比色法含量测定
DOI: 10.3724/SP.J.1145.2010.00794, PP. 794-797
Keywords: 麻疯树,脱油种仁,总生物碱,酸性染料比色法,盐酸川芎嗪
Abstract:
对不同产地麻疯树脱油种仁中的总生物碱进行提取,采用酸性染料比色法,以盐酸川芎嗪为对照品,于420nm处测定总生物碱含量,并利用单因素法考察最佳提取条件.结果表明,盐酸川芎嗪在0.036~0.180mgml-1范围内线性关系良好(r2=0.9999),平均加样回收率为98.19%,rsd为2.53%(n=6).7个不同产地麻疯树脱油种仁中总生物碱含量在3.817~4.467mgg-1之间,其中四川攀枝花地区的总生物碱含量最高.该方法操作简便,准确可靠,重复性好,可作为麻疯树脱油种仁总生物碱的含量测定方法.图2表2参15
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