|
OALib Journal期刊
ISSN: 2333-9721
费用：99美元
|
|
|
|
camoo4微晶的微波水热法可控合成
DOI: 10.3969/j.issn.1671-7627.2012.03.018, PP. 88-92
Keywords: camoo4,微波水热法,形貌
Abstract:
采用微波水热法合成出梭状、哑铃状和花状的camoo4微晶,考察ph、乙二醇(eg)与水的体积比和反应时间对产物形貌和尺寸的影响。用x线衍射仪(xrd)和扫描电镜(sem)对产物的结构形貌进行了表征。结果表明:ph为7时,合成产物为梭子状;ph为11时,合成的产物为哑铃状。随着eg加入量的增加,梭状颗粒的尺寸逐渐减小,当v(eg):v(h2o)为4:1时,得到了长轴为1μm、短轴为0.5μm的梭状camoo4粉体。另外,反应时间为3h时,可得到粒径为5μm的花状形貌的产物,并提出自组装camoo4花状形貌的形成过程。
| [1] | dingy,yush,liuc,etal.3dachitectureofironmolybdate:phaseselectivesynthesis,growthmechanism,andmagneticproperties[j].chemeurj,2007,13(3):746-753.
|
| [2] | 周立亚,王雷,龚福忠,等.camoo4超细粒子的制备及发光性能[j].广西大学学报:自然科学版,2007,32(4):394-397.
|
| [3] | ryujh,yoonjw,limcs,etal.microwave-assistedsynthesisofbariummolybdatebyacitratecomplexmethodandorientedaggregation[j].materresbull,2005,40(9):1468-1476.
|
| [4] | luozj,lihm,xiajx,etal.controlledsynthesisofdifferentmorphologiesofbawo4crystalsviaasurfactant-assistedmethod[j].jcrystgrowth,2007,300(2):523-529.
|
| [5] | 蒋文俊,张春祥,朱俊武,等.介孔纳米钼酸钡粉末的制备及表征[j].人工晶体学报,2008,37(6):1385-1389.
|
| [6] | teshimak,yubutak,sugiuras,etal.selectivegrowthofcalciummolybdatewhiskersbyrapidcoolingofasodiumchlorideflux[j].crystgrowthdes,2006,6(7):1598-1601.
|
| [7] | gongq,qianxf,caohl,etal.novelshapeevolutionofbamoo4microcrystals[j].jphyschem:b,2006,110(39):19295-19299.
|
| [8] | 徐淑雷,倪亚茹,陆春华,等.sb掺杂sno2纳米颗粒的微波辅助溶剂热合成[j].南京工业大学学报:自然科学版,2008,30(4):16-19.
|
| [9] | mikhailikvb,kraush,itohm,etal.radiativedecayofself-trappedexcitonsincamoo4andmgmoo4crystals[j].jphyscondensmatter,2005,17(46):7209-7218.
|
| [10] | wangws,zhenl,xucy,etal.roomtemperaturesynthesis,growthmechansim,photocatalyticandphotoluminescencepropertiesofcadumiummolybdatecore-shellmicrospheres[j].crystgrowthdes,2009,9(3):1558-1568.
|
| [11] | gongq,qianxf,maxd,etal.large-scalefabricationofnovelhierarchical3dcamoo4andsrmoo4mesocrystalsviaamicroemulsion-mediatedroute[j].crystgrowthdes,2006,6(8):1821-1825.
|
| [12] | luozj,lihm,shuhm,etal.synthesisofbamoo4nestlikenanostructuresunderanewgrowthmechanism[j].crystgrowthdes,2008,8(7):2275-2281.
|
| [13] | wangws,huyx,goeblj,etal.shape-andsize-controlledsynthesisofcalciummolybdatedoughnut-shapedmicrostructures[j].jphyschem:c,2009,113(37):16414-16423.
|
| [14] | wangxm,xuhy,wangh,etal.morphology-controlledbawo4powdersviaatemplate-freeprecipitationtechnique[j].jcrystgrowth,2005,284(1/2):254-261.
|
| [15] | 杨宇翔,张莉苹,邵建国,等.溶剂热合成纳米fe3o4及其性能表征[j].同济大学学报:自然科学版,2010,38(8):1205-1209.
|
| [16] | guj,zhuyc,lihb,etal.uniformln3+(eu3+,tb3+)dopednala(wo4)2nanocrystals:synthesis,characterization,andopticalproperties[j].jsolidstatechem,2010,183(3):497-503.
|
| [17] | linkl,changj,zhuyj,etal.afacileone-stepsurfactant-freeandlow-temperaturehydrothermalmethodtoprepareuniform3dstructuredcarbonatedapatiteflowers[j].crystgrowthdes,2009,9(1):177-181.
|
Full-Text
|
|
Contact Us
service@oalib.com QQ:3279437679 
WhatsApp +8615387084133
|
|
