|
OALib Journal期刊
ISSN: 2333-9721
费用：99美元
|
|
|
|
准东次烟煤中长链烷醛的富集与分析
, PP. 257-261
Keywords: 长链烷醛,准东次烟煤,分级萃取,柱层析
Abstract:
？用等体积的二硫化碳（cds）与丙酮的混合溶剂萃取了准东次烟煤得到可溶物，然后依次用石油醚（pe）和cds萃取该可溶物为pe萃取物（e1）和cds萃取物（e2）。在硅胶层析柱中依次用pe和30%的cds/pe对e2进行洗脱，富集了长链烷醛（lcnas，c18~27）并用气相色谱/质谱联用仪分析了lcnas。分级萃取和柱层析提供了从中低阶煤中富集lcnas的有效方法。lcnas可能是煤中重要的生物标志物。
| [1] | weixy,wangxh,zongzm,nizh,zhanglf,jiyf,xiekc,weeleec,liuzx,chunb,cuijy.identificationoforganochlorinesandorganobrominesincoals[j].fuel,2004,83(17/18):2435-2438.
|
| [2] | chaffeeal,fookescjr.polycyclicaromatichydrocarbonsinaustraliancoals—ⅲ.structuralelucidationbyprotonnuclearmagneticresonancespectroscopy[j].orggeochem,1988,12(3):261-271.
|
| [3] | changh-ck,nishiokam,bartlekd,wisesa,bayonajm,markideske,leeml.identificationandcomparisonoflow-molecular-weightneutralconstituentsintwodifferentcoalextracts[j].fuel,1988,67(1):45-57.
|
| [4] | hayatsur,mcbethrl,neillph,xiay,winansre.terpenoidbiomarkersinargonnepremiumcoalsamplesandtheirroleduringcoalification[j].energyfuels,1990,4(5):456-463.
|
| [5] | wangtg,simoneitbrt,philprp,yucp.extended8β(h)-drimaneand8,14-secohopaneseriesinachinesebogheadcoal[j].energyfuels,1990,4(2):177-183.
|
| [6] | shidl,weixy,chenb,zongzm,zhaoyp,fanx,houjn.theenrichmentofcondensedarenesingetingbituminouscoal[j].energysources,parta,2013,35(20):1898-1904.
|
| [7] | shidl,weixy,fanx,zongzm,chenb,zhaoyp,wangyg,caojp.characterizationsoftheextractsfromgetingbituminouscoalbyspectrometries[j].energyfuels,2013,27(7):3709-3717.
|
| [8] | wilserj,hulstag,denhartogjc.theoccurrenceofplantwaxconstituentsinairborneparticulatematterinanurbanizedarea[j].chemosphere,1982,11(11):1087-1096.
|
| [9] | gilpinja,mclaffertyfw.massspectrometricanalysisaliphaticaldehydes[j].analchem,1957,29(7):990-994.
|
| [10] | christiansenk,mahadevanv,viswanathancv,holmanrt.massspectrometryoflong-chainaliphaticaldehydes,dimethylacetalsandalk-1-enylethers[j].lipids,1969,4(6):421-427.
|
| [11] | 葛岭梅,薛韩玲,徐精彩,邓军,张辛亥.对煤分子中活性基团氧化机理的分析[j].煤炭转化,2001,24(3):23-28.
|
| [12] | (geling-mei,xuehan-ling,xujing-cai,dengjun,zhangxin-hai.studyontheoxidationmechanismofactivegroupsofcoal[j].coalconversion,2001,24(3):23-28.)
|
| [13] | lambertonj.thelong-chainaldehydesofsugar-canewax[j].austjchem,1965,18(6):911-913.
|
| [14] | kranzz,lambertonj,murrayk,redcliffea.sugar-canewax.ⅱ.anexaminationoftheconstituentsofsugar-canecuticlewaxbygaschromatography[j].austjchem,1960,13(4):498-505.
|
| [15] | cormiermj,strehlerbl.theidentificationofkcf:requirementoflong-chainaldehydesforbacterialextractluminescence[j].jamchemsoc,1953,75(19):4864-4865.
|
| [16] | strehlerbl,cormiermj.isolation,identification,andfunctionoflongchainfattyaldehydesaffectingthebacterialluciferin-luciferasereaction[j].jbiolchem,1954,211(1):213-225.
|
| [17] | graygm.theseparationofthelongchainfattyaldehydesbygas-liquidchromatography[j].jchromatogra,1960,4:52-59.
|
| [18] | o'brienjs,sampsonel.fattyacidandfattyaldehydecompositionofthemajorbrainlipidsinnormalhumangraymatter,whitematter,andmyelin[j].jlipidres,1965,6(4):545-551.
|
| [19] | prahlfg,pintola.ageochemicalstudyoflong-chainn-aldehydesinwashingtoncoastalsediments[j].geochimcosmochimacta,1987,51(6):1573-1582.
|
| [20] | albaigsj,algabaj,grimaltj.extractableandboundneutrallipidsinsomelacustrinesediments[j].orggeochem,1984,6:223-236.
|
| [21] | sunlb,zongzm,koujh,caojp,yugy,zhaow,libm,leecw,xiekc,weixy.identificationoforganicchlorinesandiodinesintheextractsfromhydrotreatedargonnepremiumcoalresidues[j].energyfuels,2007,21(4):2238-2239.
|
| [22] | dingmj,zongzm,zongy,ou-yangxd,huangyg,zhoul,wangf,caojp,weixy.isolationandidentificationoffattyacidamidesfromshenglicoal[j].energyfuels,2008,22(4):2419-2421.
|
| [23] | dingmj,liwd,xierl,zongy,caiky,pengyl,zongzm,weixy.separationandanalysisofaromatichydrocarbonsfromtwochinesecoals[j].jchinaunivmintechnol,2008,18(3):432-436.
|
| [24] | zongy,zongzm,dingmj,zhoul,huangyg,zhengyx,jinx,maym,weixy.separationandanalysisoforganiccompoundsinanerdoscoal[j].fuel,2009,88(3):469-474.
|
| [25] | weixy,wangxh,zongzm.extractionoforganonitrogencompoundsfromfivechinesecoalswithmethanol[j].energyfuels,2009,23(10):4848-4851.
|
| [26] | hazaii,alexanderg,szkelyt,essigerb,radekd.investigationofhydrocarbonconstituentsofayoungsub-bituminouscoalbygaschromatography-massspectrometry[j].jchromatogra,1986,367:117-133.
|
| [27] | zhouj,zongzm,chenb,yangzs,lip,luy,yuexm,congxs,weiyb,wangyg,fanx,zhaoyp,weixy.theenrichmentandidentificationofmethylalkanonesfromthermallysolubleshenglilignite[j].energysources,parta,2013,35(23):2218-2224.
|
| [28] | liuzw,zongzm,lijn,chencf,jiangh,pengyl,xuejq,yangxl,zhengyx,zhoux,xierl,weixy.isolationandidentificationoftwobis(2-ethylheptyl)benzenedicarboxylatesfromlingwucoal[j].energyfuels,2008,23(1):588-590.
|
| [29] | liuzw,weixy,zongzm,lijn,xuejq,chenxf,chenfj.isolationandidentificationofmethylalkanoatesfromlingwucoal[j].energyfuels,2010,24(4):2784-2786.
|
| [30] | gschwendpm,zafiriouoc,mantourarfc,schwarzenbachrp,gagosianrb.volatileorganiccompoundsatacoastalsite.1.seasonalvariations[j].environscitechnol,1982,16(1):31-38.
|
| [31] | iinom,kumagaij,itoo.coalextractionswithcarbondisulfide-n-methyl-2-pyrrolidonemixtureatroomtemperature[j].jfuelsocofjpn,1985,64(3):210-212.
|
| [32] | zongzm,pengyl,qinzh,liujz,wul,wangxh,liuzg,zhousl,weixy.reactionofn-methyl-2-pyrrolidinonewithcarbondisulfide[j].energyfuels,2000,14(3):734-735.
|
Full-Text
|
|
Contact Us
service@oalib.com QQ:3279437679 
WhatsApp +8615387084133
|
|
