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含能材料  2005 

缩水甘油硝酸酯的一锅法合成(英)

Keywords: 有机化学,含能材料,合成,缩水甘油硝酸酯,一锅法

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Abstract:

环氧氯丙烷滴加到35%的稀硝酸中,于20℃左右进行开环反应,然后用氢氧化钠溶液进行关环反应,得到缩水甘油硝酸酯,得率为60%。用FTIR,1HNMR,13CNMR和元素分析对产物进行了结构表征。

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