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含能材料  2007 

六烯丙基六氮杂异伍兹烷的合成

Keywords: 有机化学,六烯丙基六氮杂异伍兹烷,合成,CL-20

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Abstract:

以烯丙胺与乙二醛在温和条件下缩和得到了六烯丙基六氮杂异伍兹烷,用FTIR,1HNMR,13CNMR等方法对其结构进行了表征,所用合成方法比文献方法简单,收率达到37.1%。以此缩合产物作为硝化前体,采用硝-硫混酸为硝化剂试图合成出高能量密度化合物CL-20。

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