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常压制备SiO2气凝胶薄膜

Keywords: SiO2气凝胶制备薄膜硅烷化溶剂凝胶工艺压制椭偏光谱傅里叶红外光谱结构和性能

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Abstract:

采用溶胶-凝胶工艺在常压下制备了SiO2气凝胶薄膜,并用傅里叶红外光谱仪(FTIR)、扫描电子显微镜(SEM)、椭偏光谱仪等表征了薄膜的结构和性能.研究结果表明,气凝胶薄膜的折射率低达1.067,对应孔洞率为87.7%,密度为0.269×103kg·m-3,热导率为0.020W·m-1·K-1(300K)时,介电常数为1.52.这些优异性能的获得,主要归因于酸/碱两步催化、溶剂替换以及胶粒表面硅烷化等三个过程.

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