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材料工程  2011 

碳包裹镍核-壳结构复合纳米颗粒的制备及性能研究

, PP. 30-33

Keywords: 碳包覆,核-壳结构,纳米复合颗粒,阳极弧,微观结构

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Abstract:

采用自行研制的实验装置,通过阳极弧放电等离子体技术成功制备了碳包裹镍核-壳结构纳米复合颗粒,并采用酸洗和磁选的方法对初产物进行了纯化。利用高分辨透射电子显微镜(HRTEM)、X射线衍射(XRD)、透射电子显微镜(TEM)和X射线能量色散分析谱仪(XEDS)等测试手段对样品的化学成分、形貌、微观结构和粒度等特征进行了表征。结果表明阳极弧等离子体技术制备的碳包覆纳米颗粒具有明显的核(面心立方镍)-壳(无定形碳)结构,颗粒大多呈球形或椭球形,粒径分布在15~40nm范围,平均粒径为30nm,镍粒子外层碳的厚度为6~8nm。

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