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同位素  2008 

188ReN核配合物制备新方法研究

Keywords: 制备,188ReN,NEPTDD

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Abstract:

提出了以丁二酰肼（SDH）作为N给予体，SnCl2作为还原剂，加入非放ReO4-，在草酸存在下，制备产率大于95％的188Re≡N核中间体化合物。并在此基础上，制得了放化纯大于90%的新型配合物188ReN–NEPTDD（2,2,9,9-四甲基-4,7-二氮-4-乙撑哌啶-1,10-二硫癸烷），该配合物具有较好的稳定性。

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