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水相中合成磷酸三苯酯的研究

, PP. 85-87

Keywords: 水相,磷酸三苯酯,合成

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Abstract:

研究了在水相中合成磷酸三苯酯的工艺条件,找到了一条比较好的易实现工业化的合成方法,完全用水作溶剂,当n(PhOH)∶n(NaOH)∶n(POCl3)=0.90∶0.99∶0.33,反应时间为2.5h时,可使产率达到91%.

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