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西兰花状碳酸钙粉体的制备及表征

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Abstract:

以醋酸钙和碳酸钠溶液为原料,柠檬酸三钠为添加剂,采用沉淀法制备了西兰花状碳酸钙粉体。研究了柠檬酸三钠添加量和温度对制备碳酸钙粉体的影响;通过X射线衍射仪、扫描电子显微镜、红外光谱仪、热重分析表征了样品的相结构、形貌和粒度。结果表明在反应温度为40℃时,柠檬酸三钠添加量为10%(质量分数,下同)的条件下,制得了单一的、粒度为7~18μm的西兰花状碳酸钙粉体;柠檬酸三钠添加量分别为5%,15%和20%的条件下,分别得到了六边形、飞碟状、牡丹花形等特殊形貌的碳酸钙晶粒。在反应温度为20℃和柠檬酸三钠添加量为10%的条件下,制得了均匀球形碳酸钙粉体。并用多二维成核-层生长理论解释了西兰花状碳酸钙的形成机理。

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