OALib Journal期刊
ISSN: 2333-9721
费用:99美元
|
|
|
无水溶胶-凝胶法制备有机-无机杂化光波导薄膜
Abstract:
以二苯基二羟基硅烷(diphenylsilanediol,DPSD)和γ-甲基丙烯酰氧基丙基三甲氧基硅烷(γ-Methacryloxypropyltrimethoxysilane,MAPTMS)为前驱体,用无水溶胶-凝胶法合成出有机-无机杂化材料,将其旋涂在硅基片和石英玻璃片上得到杂化光波导薄膜。利用Abbe折射仪测试薄膜的折射率,用Fourier红外光谱仪和Raman光谱仪测试了薄膜的红外吸收光谱和Raman散射光谱,用紫外-可见-近红外分光光度计测试了薄膜的光吸收性质,用棱镜耦合法测试薄膜的光传输损耗。结果表明控制DPSD的加入量可以调节薄膜的折射率(1.471~1.515);杂化材料在可见和近红外区域的光透过率在90%以上;在265nm处存在强烈的苯环K带吸收峰;薄膜的光传输损耗约为1.0dB/cm。
References
[1] | 黄剑锋. 溶胶-凝胶原理与技术[M]. 北京: 化学工业出版社, 2005: 181-215. HUANG Jianfeng. The Principle and Technology of Sol-Gel (in Chinese). Beijing: Chemical Industry Press, 2005: 181-215. [2] 龚春林, 王德海. 溶胶凝胶法制备紫外光固化有机无机杂化材料的研究进展[J]. 轻工机械, 2009, 27(6): 1-4. GONG Chunlin, WANG Dehai. Light Ind Mach (in Chinese), 2009, 27(6): 1-4. [3] 葛建芳, 卢凤纪. 溶胶-凝胶法制备有机-无机反应型杂化材料[J]. 化学通报, 2002, 65: 1-7. GE Jianfang, RU Fengji. Chem Online (in Chinese), 2002, 65: 1-7. [4] 赵凤刚, 汪国年, 胡丽丽. 溶胶凝胶法稀土光波导薄膜研究进展[J]. 材料导报, 2006, 20(6): 14-17. ZHAO Fenggang, WANG Guonian, HU Lili. Mater Rev (in Chinese), 2006, 20(6): 14-17. [5] 倪克钒, 单国荣, 翁志学. 制备有机-无机杂化纳米材料的研究进展[J]. 高分子通报, 2006(11): 58-62. NI Kefan, SHAN Guorong, WENG Zhixue. Chin Polymer Bull (in Chinese), 2006(11): 58-62. [6] 张秋根, 周国波, 刘庆林. 有机-无机杂化分离膜研究进展[J]. 高分子通报, 2006(11): 52-57. ZHANG Qiugen, ZHOU Guobo, LIU Qinglin. Advances in hybrid organic-inorganic separation membranes [J]. Chin Polymer Bull (in Chinese), 2006(11): 52-57. [7] 钟敏, 赵高凌, 张溪文, 等. 有机/无机纳米复合材料的制备及应用[J]. 材料科学与工程, 2000, (18): 369-371. ZHONG Min, ZHAO Gaoling, ZHANG Xiwen, et al. Mater Sci Eng (in Chinese), 2000 (18): 369-371. [8] PORTIERA J, CHOYB J H, Subramanianc. Inoganic-organic hybrids as precursors to functional materials [J]. Int J Inorg Mater, 2001 (3): 581-592. [9] KHIMICH N N. Synthesis of silica gels and organic-inorganic hybrids on their base [J]. Glass Phys Chem, 2004, 5(30): 430-442. [10] 刘冰, 强亮生. 溶胶-凝胶法制备光学杂化功能材料[J]. 化学进展, 2005, 17(1): 85-89. LIU Bing, QIANG Liangsheng. Progress of organic-inorganic hybrid optical-functional materials prepared by the sol-gel method [J]. Pro in Chemis (in Chinese), 2005, 17(1): 85-89. [11] DUAN L O, ANGELA B. Seddon.Near and mid-infrared spectroscopy of sol-gel derived ormosils: vinyl and phenyl silicates [J]. J Non-Cryst Sol, 1997, 210(2): 187-203. [12] JANA S, LIM M A, In Chan Baek, et al. Non-hydrolytic sol-gel synthesis of epoxysilane-based inorganic-organic hybrid resins [J]. Mater Chem Phys, 2008 (112): 1008-1014. [13] 郑顺旋. 激光拉曼光谱学[M]. 上海: 上海科学技术出版社, 1985: 252-267. ZHENG Shunxuan. Laser-Raman spectroscopy (in Chinese). Shanghai: Shanghai Scientific and Technologic Press, 1985: 252-267. [14] KIM J S, YANG S C, BAE B S. Thermal stability of sol-gel derived methacrylate oligosiloxane-based hybrids for LED encapsulants [J]. J Sol-Gel Sci Technol, 2010 (53): 434-440. [15] 贾凌华, 邱枫, 钱颖, 等. 数码照相法测量离子交换平面光波导损耗特性[J]. 光子学报, 2009, 38(5): 1058-1061. JIA Linghua, QIU Feng, QIAN Ying, et al. Digital camera photographing in measuring propagation loss properties of ion-exchange planar optical waveguides [J]. Acta Photon Sin, 2009, 38(5): 1058- 1061. [16] ALMEIDA R M, MORAIS P J, VASCONCELOS H C. Optical loss mechanisms in nanocomposite sol-gel planar waveguides [C]. Proc SPIE, 1997 (3136): 296-303.
|
Full-Text
|
|
Contact Us
service@oalib.com QQ:3279437679 
WhatsApp +8615387084133
|
|