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OALib Journal期刊
ISSN: 2333-9721
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Al-Mg-Si合金搅拌摩擦焊接头DSC测试过程中组织变化及能量释放分析*
DOI: 10.3724/SP.J.1037.2013.00419, PP. 587-593
Keywords: 搅拌摩擦焊,(FSW),电子背散射技术,(EBSD),储存能,Al-Mg-Si合金,差热扫描量热法,(DSC)
Abstract:
对Al-Mg-Si合金搅拌摩擦焊焊核区组织进行了差热扫描量热分析(DSC),同时运用EBSD和TEM观察了焊核区的微观组织,并对存储能进行了定量分析.研究表明,焊核区为不稳定组织,焊核区组织中小角度晶界占42%,大角度晶界占58%,同时晶粒内部分布有较高密度的位错结构.焊核区含有较高的存储能(8.565J/g),通过EBSD对焊核区较高存储能进行了定量分析,结果表明,位错存储在晶界和亚晶界的能量为0.0247J/g,存储在晶粒内部的能量为0.0712J/g.通过DSC定量分析的能量释放来自于焊核区晶粒内部位错的消失和析出相的析出,其中由析出相析出所造成的能量释放占主导作用,位错存储在晶界和亚晶界的存储能通过DSC加热并未释放.
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