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化学进展  2015 

外界刺激调控的表面引发原子转移自由基聚合

DOI: 10.7536/PC140804, PP. 146-156

Keywords: 表面引发聚合,原子转移自由基聚合(ATRP),聚合物刷,外界调控

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Abstract:

聚合物刷被广泛用于调控表/界面的物理化学性质,表面引发聚合(SIP)是制备聚合物刷的有效手段,该方法已广泛地用于合成具有各种结构以及功能的聚合物以及无机/有机杂化材料。表面引发原子转移自由基聚合(SI-ATRP)方法是表面接枝聚合刷最为常用的方法,但是目前的方法存在很多问题,例如单体利用率低、反应条件苛刻、可控性较差等。近年来,一些研究组发展了一系列通过外界刺激来调控聚合过程的新方法,旨在克服以上缺陷。本文首先详细介绍了SI-ATRP的机理,在此基础上讨论通过一系列外界刺激(电化学、光、化学试剂等)灵活调控表面引发-原子转移自由基聚合来制备聚合物刷的最新研究进展,同时展望利用新的聚合方法调控聚合物刷结构、界面性质以及应用。

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