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化学进展  2012 

硅胶基质高效液相色谱填料研究进展

, PP. 122-130

Keywords: 高效液相色谱,硅胶,填料

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Abstract:

高效液相色谱(HPLC)不仅是一种有效的分析分离手段,也是一种重要的高效制备分离技术。色谱柱是HPLC系统的核心,不同性能的填料是HPLC广泛应用的基础。硅胶是开发最早、研究最为深入、应用最为广泛的HPLC固定相基质,其制备方法主要有喷雾干燥法、溶胶-凝胶法、聚合诱导胶体凝聚法及模板法等。近年来,亚2μm小粒径硅胶、核-壳型硅胶、双孔径硅胶、介孔性硅胶、有机杂化硅胶等新型硅胶应用于HPLC并取得了色谱分离技术的飞速发展,例如基于亚2μm填料的超高压液相色谱技术、基于核-壳型填料的快速分离技术、基于杂化硅胶填料的高温液相色谱技术等。硅胶经表面化学键合、聚合物包覆等有机改性可制得先进的大分子限进填料、温敏性填料、手性填料等,大大扩展了HPLC的应用范围。本文对液相色谱用硅胶的制备方法、改性与修饰方法以及硅胶基质固定相的评价方法加以系统综述,概述了新型硅胶在HPLC中的应用进展,并对硅胶基质填料的发展方向与应用前景进行了展望。

 References

[1]  Unger K K, Skudas R, Schulte M M. J. Chromatogr. A, 2008, 1184: 393-415
[2]  Nawrocki J, Dunlap C, Mccormick A, Carr P W. J. Chromatogr. A, 2004, 1028: 1-30
[3]  Huai Q Y, Wang X L, Zuo Y M. Chromatographia, 2002, 55: 637-645
[4]  Kirkland J J, DeStefano J J. J. Chromatogr. A, 2006, 1126: 50-57
[5]  West C, Elfakir C, Lafosse M. J. Chromatogr. A, 2010, 1217: 3201-3216
[6]  Pelletier S, Lucy C A. J. Chromatogr. A, 2006, 1125: 189-194
[7]  Pesek J J, Matyska M T. J. Sep. Sci. , 2009, 32: 3999-4011
[8]  佟巍(Tong W), 张养军(Zhang Y J), 秦伟捷(Qin W J), 钱小红(Qian X H). 色谱(Chinese of Chromatography), 2010, 28(10): 915-922
[9]  Rahman I A, Vejayakumaran P, Sipaut C S, Ismail J, Baker M A, Adnan R, Chee C K. Ceram. Int. , 2006, 32: 691-699
[10]  Wang X D, Shen Z X, Sang T, Cheng X B, Li M F, Chen L Y. J. Colloid Interface Sci. , 2010, 341: 23-29
[11]  Bhagat S D, Rao A V. Appl. Surf. Sci., 2006, 252: 4289-4297
[12]  Rao A V, Bhagat S D. Solid State Sci., 2004, 6: 945-952
[13]  Choi D G, Yang S M. J. Colloid Interf. Sci., 2003, 261: 127-132
[14]  赵贝贝(Zhao B B), 许婵婵(Xu C C), 唐涛(Tang T), 李彤(Li T), 张维冰(Zhang W B), 王风云(Wang F Y). 无机材料学报(Chinese of Journal of Inorganic Materials), 2011, 26: 1090-1094
[15]  Poyraz A S, Albayrak C, Dag O. Microporous Mesoporous Mater., 2008, 115: 548-555
[16]  Li Y Y, Cheng S Y, Dai P C, Liang X M, Ke Y X. Chem. Commun., 2009, 1085-1087
[17]  Hao W Q, Di B, Liu H, Hang T J, Yan F, Su M X. Chromatographia, 2011, 73: 623-629
[18]  Wan H H, Liu L, Li C M, Xue X Y, Liang X M. J. Colloid Interf. Sci., 2009, 337: 420-426
[19]  Liu X B, Li L S, Du Y, Guo Z, Ong T T, Chen Y, Ng S C, Yang Y H. J. Chromatogr. A, 2009, 1216: 7767-7773
[20]  Ai F, Li L S, Ng S C, Tan T T Y. J. Chromatogr. A, 2010, 1217: 7502-7506
[21]  Yang L M, Wang Y J, Sun Y W, Luo G S, Dai Y Y. J. Colloid Interf. Sci., 2006, 299: 823-830
[22]  Yang L M, Wang Y J, Luo G S, Dai Y Y. Particuology, 2008, 6: 143-148
[23]  Kirkland J J, Truszkowski F A, Ricker R D. J. Chromatogr. A, 2002, 965: 25-34
[24]  Faria A M, Magalhaes D R, Collins K E, Collins C H. Anal. Chim. Acta, 2005, 550: 137-143
[25]  Novakova L, Matysova L, Solich P. Talanta, 2006, 68: 908-918
[26]  Jiang Z P, Fisk R P, Gara J O, Walter T H, Wyndham K D. US 2007/0243383, 2007
[27]  Guo R R, Ding M Y. Colloids Surf. A, 2007, 292: 153-158
[28]  Li Y S, Li B, Han N Y, Xu B J. J. Chromatogr. A, 2003, 1021: 183-189
[29]  Kirkland J J. J. Chromatogr. A, 2004, 1060: 9-21
[30]  Luo H, Carr P W. Anal. Bioanal. Chem., 2008, 391: 919-923
[31]  He Z Y, Lv C G, Fan X X, Zhou Z Q. Anal. Chim. Acta, 2011, 689(1): 143-148
[32]  Mallik A K, Rahman M M, Czaun M, Takafuji M, Ihara H. J. Chromatogr. A, 2008, 1187: 119-127
[33]  Sadilek P, Satinsky D, Solich P. Trends Anal. Chem., 2007, 26: 375-384
[34]  Kurpczynska K, Buszewski B, Jandera P. Anal. Chem., 2004, 76: 227-234
[35]  Buszewski B, Bocian S, Felinger A. J. Chromatogr. A, 2008, 1191: 72-77
[36]  Dehouck P, Visky D, Heyden Y V, Adams E, Kovacs Z, Noszal B, Massart D L, Hoogmartens J. J. Chromatogr. A, 2004, 1025: 189-200
[37]  Visky D, Heyden Y V, Ivanyi T, Baten P, Beer J D, Kovacs Z, Noszal B, Dehouck P, Roets E, Massart D L, Hoogmartens J. J. Chromatogr. A, 2003, 1012: 11-29
[38]  Ye C, Terfloth G, Li Y, Kord A. J. Pharm. Biomed. Anal., 2009, 50: 429-431
[39]  Claessens H A, Straten M A. J. Chromatogr. A, 2004, 1060: 23-41
[40]  Liu Y, Grinberg N, Thompson K C, Wenslow R M, Neue U D, Morrison D, Walter T H, Gara J E O, Wyndham K D. Anal. Chim. Acta, 2005, 554: 144-151
[41]  Neue U D. J. Sep. Sci., 2007, 30: 1611-1627
[42]  Wu N, Liu Y, Lee M L. J. Chromatogr. A, 2006, 1131: 142-150
[43]  Lurie I S. J. Chromatogr. A, 2005, 1100: 168-175
[44]  Klejdus B, Vacek J, Lojkova L, Lojkova L, Benesova L, Kuban V. J. Chromatogr. A, 2008, 1195: 52-59
[45]  Liu Y, Grinberg N, Thompson K C, Wenslow R M, Neue U D, Morrison D, Walter T H, OGara J E, Wyndham K D. Anal. Chim. Acta, 2005, 554: 144-151
[46]  Teutenberg T. Anal. Chim. Acta, 2009, 643: 1-12
[47]  Lurie I, Li L. J. Liq. Chromatogr. Related Technol. , 2009, 32: 2615-2626
[48]  Paek C, McCormick A V, Carr P W. J. Chromatogr. A, 2010, 1217: 6475-6483
[49]  Ai F, Li L, Ng S C, Tan T T Y. J. Chromatogr. A, 2010, 1217: 7502-7506
[50]  Unger K K, Kumar D, Grun M, Buchel G, Ludtke S, Adam T, Schumacher K, Renker S. J. Chromatogr. A, 2000, 892: 47-55
[51]  Uzun L, Yavuz H, Say R. Ind. Eng. Chem. Res. , 2004, 43: 6507-6513
[52]  Haginaka J. J. Chromatogr. B, 2008, 866: 3-13
[53]  Davies N H, Euerby M R, McCaller D V. J. Chromatogr. A, 2008, 1178: 71-78
[54]  Qiu H D, Liang X J, Sun M, Jiang S X. Anal. Bioanal. Chem., 2011, 399: 3307-3322
[55]  Kang Y J, Shan W, Wu J Y. Chem. Mater. , 2006, 18(7): 1861-1866
[56]  Zhao L, Yu J G, Guo R, Cheng B. Key Eng. Mater., 2005, 280/283: 1153-1156
[57]  张庆合(Zhang Q H). 大连化学物理研究所博士后出站报告(Post Doctoral Dissertation of Dalian Institute of Chemical Physics Chinese of Academy of Sciences), 2002
[58]  Chang S M, Lee M, Kim W S. J. Colloid Interface Sci. , 2005, 286: 536-542
[59]  Zhao B B, Tian C H, Zhang Y, Tang T, Wang F Y. Particuology, 2011, 9: 314-317
[60]  Hohenesche C F, Ehwald V, Unger K K. J. Chromatogr. A, 2004, 1025: 177-187
[61]  杨新立(Yang X L). 中国科学院大连化学物理研究所博士论文(Doctoral Disseratation of Dalian Institute of Chemical Physics Chinese of Academy of Sciences), 2001
[62]  赵贝贝(Zhao B B), 许婵婵(Xu C C), 唐涛(Tang T), 李彤(Li T), 张维冰(Zhang W B), 王风云(Wang F Y). 分析化学(Chinese of Analytical Chemistry), 2011, 39: 1243-1246
[63]  Wu Y J, Ren X Q, Wang J. Mater. Chem. Phys. , 2009, 113: 773-779
[64]  Tian R J, Sun J M, Zhang H, Ye M L, Xie C H, Dong J, Hu J W, Ma D, Bao X H, Zou H F. Electrophoresis, 2006, 27: 742-748
[65]  Kirkland J J, Truszkowski F A, Dilks J C H, Engel G S. J. Chromatogr. A, 2000, 890: 3-13
[66]  Silva C R, Airoldi C, Collins K E, Collins C H. J. Chromatogr. A, 2008, 1191: 90-98
[67]  Collins C H, Silva C R, Faria A M, Collins K E, Jardim I C S F. J. Braz. Chem. Soc., 2009, 20: 604-612
[68]  Liang X, Liu S, Liu H, Liu X, Jiang S. J. Sep. Sci., 2010, 33: 3304-3312
[69]  Nakanishi K, Minakuchi H, Soga N, Tanaka N. J. Sol-Gel Sci. Technol., 1998, 13: 163-169
[70]  Wei J X, Shi Z G, Chen F, Feng Y Q, Guo Q Z. J. Chromatogr. A, 2009, 1216: 7388-7393
[71]  McCalley D V. J. Chromatogr. A, 2010, 1217: 858-880
[72]  Chice J, Meca S, Companyo R, Prat M D, Granados M. J. Chromatogr. A, 2008, 1181: 1-8
[73]  Tello A M, Lebron-Aguilar R, Quintanilla-Lopez J E, Santiuste J M. J. Chromatogr. A, 2009, 1216: 1630-1639
[74]  Tamayo F G, Titirici M M, Martin-Esteban A, Sellergren B. Anal. Chim. Acta, 2005, 542: 38-46
[75]  Burdukova E, Li H, Ishida N, Shea J P O, Franks G V. J. Colloid Interf. Sci. , 2010, 342: 586-592
[76]  Kanazawa H, Ayano E, Sakamoto C, Yoda R, Kikuchi A, Okano T. J. Chromatogr. A, 2006, 1106: 152-158
[77]  Faria A M, Magalhaes D R, Collins K E, Collins C H. Anal. Chim. Acta, 2005, 550: 137-143
[78]  Xiong C Q, Zhou X Y, Chen R, Zhang Y M, Peng W P, Nie Z X, Chang H C, Liu H W, Chen Y. Anal. Chem., 2011, 83: 5400-5406
[79]  Standard Reference Materia？869a. National Institute of Standard & Technology, 2002
[80]  Standard Reference Materia？870a. National Institute of Standard & Technology, 2002
[81]  Nguyen D T T, Guillarme D, Rudaz S, Veuthey J L. J. Sep. Sci., 2006, 29: 1836-1848
[82]  Garcia-Canas V, Lorbetskie B, Girard M. J. Chromatogr. A, 2006, 1123: 225-232
[83]  Klejdus B, Vacek J, Lojkova L, Benesova L, Kuban V. J. Chromatogr. A, 2008, 1195: 52-59
[84]  Gosetti F, Frascarolo P, Polati S, Medana C, Gianotti V, Palma P, Aigotti R, Baiocchi C, Gennaro M C. Food Chem., 2007, 105: 1738-1747
[85]  Pesek J J, Matyska M T, Sukul D. J. Chromatogr. A, 2008, 1191: 136-140
[86]  Naeem H A, Sapirstein H. J. Cereal Sci., 2007, 46: 157-168
[87]  Gritti F, Guiochon G. J. Chromatogr. A, 2007, 1166: 30-46
[88]  Abrahim A, Al-Sayah M, Skrdla P, Bereznitsk Y, Chen Y, Wu N. J. Pharm. Biomed. Anal., 2010, 51: 131-137
[89]  Nguyen D T T, Guillarme D, Heinisch S, Marie-Pierre B, Rocca J L, Rudaz S, Veuthey J L. J. Chromatogr. A, 2007, 1167: 76-84

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