全部 标题 作者
关键词 摘要

OALib Journal期刊
ISSN: 2333-9721
费用:99美元

查看量下载量

相关文章

更多...
分析化学  2011 

脉冲熔融-飞行时间质谱法测定金属材料中氧、氮、氢和氩

, PP. 1555-1560

Keywords: 脉冲熔融-飞行时间质谱法,,,,

Full-Text   Cite this paper   Add to My Lib

Abstract:

采用自主研制的脉冲熔融-飞行时间质谱法可以同时测定金属中O,N,H和Ar。重点讨论质谱谱线的选择,信号获得以及数据处理和校准,并给出O,N,H和Ar4种的检出限分别为0.021,0.060,0.002和0.002μg/g,线性范围分别为0.070~500μg/g,0.200~400μg/g,0.006~40μg/g和0.005~15μg/g。并利用不同样品对本方法的准确性和精密度进行了验证,实验结果与传统方法吻合。实验表明,本方法准确、有效,可同时测定4种气体元素O,N,H和Ar。

References

[1]  1 GB/T 11261-2006,Steel and Iron-Determination of Oxygen Content-The Pulse Heating Inert Gas Fusion-InfraredAbsorption Method(钢铁氧含量的测定脉冲加热惰气熔融-红外线吸收法).National Standards of the People′sRepublic of China(中华人民共和国国家标准)
[2]  2 GB/T 20124-2006,Steel and Iron-Determination of Nitrogen Content-Thermal Conductimetric Method AfterFusion in a Current of Iinert Gas(钢铁氮含量的测定惰性气体熔融热导法).National Standards of the People′sRepublic of China(中华人民共和国国家标准)
[3]  3 GB/T 223.82-2007,Steel and Iron-Determination of Hydrogen Content-Inert Gas Impulse Fusion Heat Conduc-tivityMethod(钢铁氢含量的测定惰气脉冲熔融热导法).National Standards of the People′s Republic of China(中华人民共和国国家标准)
[4]  5 ZHU Yue-Jin,WANG Qiang,GENG Xiao-Ying(朱跃进,王强,耿小颖).Metallurgical Analysis(冶金分析),2008,28(Suppl.2):1041~1043
[5]  8 HU Shao-Cheng,SHEN Xue-Jing,WANG Peng(胡少成,沈学静,王蓬).Metallurgical Analysis(冶金分析),2010,30:805~810
[6]  11 WANG Peng,SHEN Xue-Jing,HU Shao-Cheng,YANG Zhi-Gang,MA Hong-Quan,WANG Hai-Zhou,GAOWei,ZHOU Zhen(王蓬,沈学静,胡少成,杨植岗,马红权,王海舟,高伟,周振).Metallurgical Analysis(冶金分析),2008,28(Suppl.1):109~119
[7]  13 GAO Wei,HUANG Zheng-Xu,ZHOU Zhen(高伟,黄正旭,周振).Mass Spectrom.Soc.(质谱学报),2008,29:209-212,217
[8]  16 LI Qing-Jiang,SUN Zhao-Lin,LI Nan,LI Yao-Li,ZHOU Zhen,XU Xin(李清江,孙兆林,李楠,李耀立,周振,徐欣).Mass Spectrom.Soc.(质谱学报),2010,31:28~31
[9]  4 TANG Quan-Min,ZHANG Zhu-Hui,WANG Wen-Yan(唐权民,张祖辉,王文焱).Spectrom.Lab.(光谱实验室),2006,23:503~505
[10]  6 WANG Hai-Zhou,SHEN Xue-Jing,WANG Peng(王海舟,沈学静,王蓬).China Patent(中国专利),CN101144794,2008-03-19
[11]  7 HU Shao-Cheng,SHEN Xue-Jing,WANG Peng(胡少成,沈学静,王蓬).Metallurgical Analysis(冶金分析),2009,29:34~40
[12]  9 Shen X,Wang P,Hu S.Talanta,2011,84:1057~1061
[13]  10 Gao W,Huang Z X,Nian H Q,Shen X J,Wang P,Li M,Cheng P,Dong J G,Xu X,Zhou Z.Inter.J.MassSpectrom.,2010,294:77~82
[14]  12 Wang H Z,Wang P,Shen X J,Yang Z G,Yan Y X,Hu S C,Ma H Q,Li H W.USA Patent,US 7847242B2
[15]  14 GAO Wei,FU Zhong,ZHOU Zhen(高伟,傅忠,周振).Metallurgical Analysis(冶金分析),2008,28:966~970
[16]  15 GUO Chang-Juan,GAO Wei,ZHOU Zhen(郭长娟,高伟,周振).Journal of Instrumental Analysis(分析测试学报),2008,27:339~343

Full-Text

Contact Us

service@oalib.com

QQ:3279437679

WhatsApp +8615387084133