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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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加速溶剂萃取凝胶渗透色谱/固相萃取净化气相色谱质谱法测定咸鱼中有机磷农药残留
, PP. 67-71
Keywords: 加速溶剂萃取,凝胶渗透色谱,固相萃取,气相色谱-质谱,有机磷,咸鱼
Abstract:
建立了咸鱼中有机磷农药残留的分析方法。乙腈为溶剂,样品经ASE萃取,提取液用凝胶渗透色谱除去脂类、蛋白质和大部分的色素,再经Carb/PSA小柱净化。采用GC-MS定性分析,GC-FPD定量分析。加标水平为0.05～0.20mg/kg时,农药的回收率为64.5%～98.6%,相对标准偏差2.7%～14.7%。方法的检出限为0.6～9.0μg/kg(以3倍性噪比计)。本方法具有提取效率高,净化效果好,回收率高,准确灵敏等优点,适用于咸鱼中农药残留检测实际工作的需要。
| [1] | Cheng X H,Zhang Z J,Tian S K.Spectrochim.Acta Part A,2007,67(5):1270～1275
|
| [2] | RAO Zhi-Ming,WANG Jian-Ning,LI Long-Di,HANG Xin-Rong(饶志明,王建宁,李隆弟,张新荣).Chinese J.Anal.Chem.(分析化学),2001,29(4):373～377
|
| [3] | Ni Y N,Qiu P,Kokot S.Anal.Chirn.Acta,2004,516(1-2):7～17
|
| [4] | Zhou L,Luo Z,Wang S M,Hui Y,Chen X G.J.Chromatogr.A,2007,1149(2):377～384
|
| [5] | HUANG Xing-Jiu,WANG Lion-Chao,SUN Yu-Feng,MENG Fan-Li,LIU Jin-Huai(黄行九,王连超,孙宇峰,孟凡利,刘锦准).Chinese J.Anal.Chem.(分析化学),2005,33(3):363～365
|
| [6] | Zhao E C,Zhao W T,Han L J,Jiang S R,Zhou Z Q.J.Chromatogr.A,2007,1175(1):137～140
|
| [7] | ZHAO Xiao-Meng,YU Tong-Quan,ZHU Gao-Qun,LU Ping,YANG Liu,WANG Shu-Ying,WANG Jian-Li(赵晓萌,于同泉,朱高群,路苹,杨柳,王淑英,王建立).Chinese Journal of Chromatography(色谱),2005,23(3):328
|
| [8] | LIU Yong-Jian,MOU Shi-Fen(刘勇建,牟世芬).Environmental Chemistry(环境化学),2002,21(4):410～411
|
| [9] | WU Gang,BAO Xiao-Xia,WANG Hua-Xiong,YU Chun-Yon,WU Hui-Ming,YE Qing-Fu(吴刚,鲍晓霞,王华雄,俞春燕,吴慧明,叶庆富).Chinese Journal of Chromatography(色谱),2008,26(5):577～582
|
| [10] | ZHU Xiao-Lan,CAI Ji-Bao,YANG Jun,SU Qing-De(朱晓兰,蔡继宝,杨俊,苏庆德).Chinese J.Anal.Chem.(分析化学),2005,33(6):821～824
|
| [11] | SU Jian-Feng(苏建峰).Chinese J.Inst.Ahal.(分析测试学报),2008,27(12):1298～1302
|
| [12] | Jin S Y,Xu Z C,Chen J P,Liang X M,Wu Y N,Qian X H.Anal.Chim.Acta,2004,523(1):117～123
|
| [13] | Li B X.He Y Z,Xu C L.Talanta,2007,72(1):223～230
|
| [14] | Garcia-Ruiz C,(A)lvarez-Llamas G,Puerto (A),Blanco E,Sanz-Medel A,Marina M L Anal.Chim.Acta,2005,543(1-2):77～83
|
| [15] | QIAN Li-Li YOH-Zhao,HU Yan-Yun(钱立立,何友昭,胡艳云).Chinese J.Anal.Chem.(分析化学),2006,34(11):1591～1594
|
| [16] | ZHAO Jie,WANG Heng,CHEN Qing-Dong,CHEN Zhi-Wei,LUAN Wei(赵洁,王恒,陈庆东,陈志伟,栾伟).Chinese.J.Anal.Chem.(分析化学),2009,37(3):351～356
|
| [17] | Padrón-Sanz C,Halko R,Sosa-Ferrera Z,Santana-Rodriguez J J.J.Chromatogr.A,2005,1078(1-2):13～21
|
| [18] | WAN Yi-Qun,LI Yan-Xia(万益群,李艳霞).Chinese J.Inst.Anal.(分析测试学报),2005,24(3):90～94
|
| [19] | Garcia-Valcárcel A I,Tadeo J L.Ahal.Chim.Acta,2009,641(1-2):117～123
|
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