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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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低压下碱金属碳酸盐催化一步法合成碳酸二甲酯
DOI: 10.1016/S1872-2067(14)60309-0, PP. 1136-1141
Keywords: 碳酸二甲酯,环氧化物,碱金属碳酸盐,一步法,低压
Abstract:
？报道了低压下碱金属碳酸盐催化环氧化物、CO2和甲醇一步合成碳酸二甲酯(DMC)的方法,系统考察了反应条件对一步合成DMC的影响规律.在最优反应条件下(初始压力0.5MPa,反应温度120℃,碳酸钠7.5mol%),以环氧乙烷为起始剂的DMC收率达到63.5%.提出了碱金属碳酸盐催化一步法合成DMC的可能反应机理.
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