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催化学报  2015 

Acetylationofalcoholsandphenolsundersolvent-freeconditionsusingironzirconiumphosphate

DOI: 10.1016/S1872-2067(14)60280-1, PP. 595-602

Keywords: Ironzirconiumphosphate,Nanoparticle,Acetylation,Alcohol,Phenol,Solvent-freecondition,Solidcatalyst

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Abstract:

？Ironzirconiumphosphate(ZPFe)nanoparticleswerefoundtofunctionasanefficientcatalystfortheacetylationofawiderangeofalcoholsandphenolsusingaceticanhydride,generatinggoodtoexcellentyieldsundersolvent-freeconditions.Thestericandelectronicpropertiesofvarioussubstrateshadasignificantinfluenceonthereactionconditionsrequiredtoachievetheacetylation.Thecatalystusedinthecurrentstudywascharacterizedbyinductivelycoupledplasma-opticalemissionspectrometry,X-raydiffraction,N2adsorption-desorption,scanningelectronmicroscopy,andtransmissionelectronmicroscopy.Theseanalysesrevealedthattheinterlayerdistanceinthecatalystincreasedfrom7.5to9.3？whenFe3+wasintercalatedbetweenthelayers,whereasthecrystallinityofthematerialwasreduced.Thisnanocatalystcouldalsoberecoveredandreusedatleastsixtimeswithoutanydiscernibledecreaseinitscatalyticactivity.Thisnewmethodfortheacetylationofalcoholsandphenolshasseveralimportantadvantages,includingmildandenvironmentallyfriendlyreactionconditions,aswellasgoodtoexcellentyieldsandafacilework-up.

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