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OALib Journal期刊
ISSN: 2333-9721
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Fe3O4@MCM-48-SO3H:Anefficientmagneticallyseparablenanocatalystforthesynthesisofbenzo[f]chromeno[2,3-d]pyrimidinones
DOI: 10.1016/S1872-2067(14)60286-2, PP. 572-578
Keywords: Mesoporousmagneticnanoparticle,Benzo[f]chromene,Chromeno[2,3-d]pyrimidine,Fe3O4@MCM-48-SO3H,Fe3O4@SiO2-SO3H
Abstract:
？Sulfonicacidgroupsweregraftedontothreedifferenttypesofsynthesizedmagneticnanoparticles,namelyFe3O4,Fe3O4@SiO2,andFe3O4@MCM-48.Thesulfonicacid-functionalizednanoparticleswereevaluatedascatalystsforthesynthesisof5-aryl-1H-benzo[f]chromeno[2,3-d]pyrimidine-2,4(3H,5H)-dionederivativesintermsofactivityandrecyclability.Theircatalyticactivitieswerecomparedwiththatofthehomogeneousacidcatalyst1-methylimidazoliumhydrogensulfate([HMIm][HSO4]).TheactivityofFe3O4@MCM-48-SO3Hwascomparabletothoseoftheotherheterogeneousandhomogeneouscatalysts.
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