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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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SuzukiReactionofArylBromidesUsingaPhosphine-FreeMagneticNanoparticle-SupportedPalladiumCatalyst
DOI: 10.1016/S1872-2067(10)60270-7, PP. 1667-1676
Keywords: superparamagneticnanoparticle,Suzukireaction,palladium,arylbromide
Abstract:
？Apalladiumcatalystimmobilizedonsuperparaganeticnanoparticleswaspreparedwithapalladiumloadingof0.30mmol/g.ThecatalystwascharacterizedusingX-raydiffraction,scanningelectronmicroscopy,transmissionelectronmicroscopy,vibratingsamplemagnetometry,thermogravimetricanalysis,Fouriertransforminfrared,atomicabsorptionspectrophotometry,andnitrogenadsorption.TheimmobilizedpalladiumcatalystwasanefficientcatalystwithoutaddedphosphineligandsfortheSuzukicross-couplingreactionofseveralarylbromideswithphenylboronicacid.Therecoveryofcatalystwassimplybymagneticdecantationinthepresenceofamagnet.Theimmobilizedpalladiumcatalystcanbereusedmanytimeswithoutsignificantdegradationincatalyticactivity.Noleachingofactivepalladiumspeciesintothereactionsolutionwasdetected.
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