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OALib Journal期刊
ISSN: 2333-9721
费用：99美元
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One-PotFour-ComponentDakin-WestSynthesisofβ-AcetamidoKetonesCatalyzedbyaVanadium-SubstitutedHeteropolyacid
DOI: 10.1016/S1872-2067(11)60379-3, PP. 923-932
Keywords: homogeneouscatalysis,heteropolyacid,Keggin,Wells-Dawson,Dakin-West,β-acetamidoketone
Abstract:
？Themulticomponentcondensationofanarylaldehyde,acetylchloride,acetonitrile,andenolizableketoneasone-potsynthesisofβ-acetamidoketonesinhighyieldswasinvestigatedusingcommercial,non-corrosive,andenvironmentallybenignKegginandWells-Dawsonheteropolyacidcatalysts.ThebestcatalystwasH5PW10V2O40.Themethodologyusedsimpleexperimentalconditions,andtheshortreactiontimesandhighyieldsindicateitisausefulstrategyforthelargescalesynthesisofβ-acetamidoketones.
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