全部 标题 作者
关键词 摘要

OALib Journal期刊
ISSN: 2333-9721
费用:99美元

查看量下载量

相关文章

更多...
科学通报  2011 

氧氯化锑的形貌转变:从束状到准圆形

, PP. 1987-1992

Keywords: 氯氧化锑,束状,准圆片,晶体分裂,形貌转变

Full-Text   Cite this paper   Add to My Lib

Abstract:

在室温下的溶液中以温和易行的实验条件,成功制备了各种形貌不同的氯氧化锑,包括束状、菱形片状、类似树叶的椭圆状和准圆片状.利用X射线衍射(XRD),扫描电子显微镜(SEM)和透射电子显微镜(TEM)等手段对制备的各种不同形貌和结构的样品进行了表征.在此基础上,提出了可能的形成机理.

References

[1]  9 Costa L, Paganetto G, Bertelli G, et al. Thermal decomposition of antimony oxyhalides: I. Oxychlorides. J Therm Anal, 1990, 36:1141-1153??
[2]  10 Chen X Y, Huh H S, Lee S W. Hydrothermal synthesis of antimony oxychloride and oxide nanocrystals: Sb4O5Cl2, Sb8O11Cl2, and Sb2O3.J Solid State Chem, 2009, 181: 2127-2132
[3]  11 Tang J J, Wang Y, Jiao Z, et al. Self-assembly nanostructures of one-dimensional antimony oxide and oxychloride. Mater Lett, 2009, 63:1481-1484??
[4]  12 Li B J, Zhao Y B, Xu X M, et al. A simple method for the preparation of containing Sb nano-and microcrystallines via an ultrasoundagitation. Ultraso Sonochem, 2007, 14: 557-562??
[5]  13 Sui Y M, Fu W Y, Yang H B, et al. Low temperature synthesis of Cu2O crystals: Shape evolution and growth mechanism. Cryst GrowthDes, 2010, 10: 99-108??
[6]  14 Wang H H, Tian F, Li X P, et al. Preparation and shape evolution of cuprous oxide in the solution phases of copper (II) dodecyl sulfate.Powder Technol, 2010, 197: 298-302??
[7]  17 Li L S, Sun N J, Huang Y Y, et al. Topotactic transformation of single-crystalline precursor discs into disc-Like Bi2S3 nanorod networks.Adv Funct Mater, 2008, 18: 1194-1201??
[8]  18 Tian L, Tan H Y, Vittal J J. Morphology-controlled synthesis of Bi2S3 nanomaterials via singleand multiple-source approaches. CrystGrowth Des, 2008, 8: 734-738
[9]  19 Hu Y H, Chen K Z. Crystal splitting in the growth of β-FeO(OH). J Cryst Growth, 2007, 308: 185-188??
[10]  20 Luo Z J, Li H M, Xia J X, et al. Controlled synthesis of different morphologies of BaWO4 crystals via a surfactant-assisted method. JCryst Growth, 2007, 300: 523-529??
[11]  22 Deng H, Liu C M, Yang S H, et al. Additive-mediated splitting of lanthanide orthovanadate nanocrystals in water: Morphological evolutionfrom Rods to sheaves and to spherulites. Cryst Growth Des, 2008, 8: 4432-4439??
[12]  23 Chen G Y, Dneg B, Cai G B, et al. The fractal splitting growth of Sb2S3 and Sb2Se3 hierarchical nanostructures. J Phys Chem C, 2008, 112:672-679??
[13]  27 Kim S, Lee J S, Mitterbauer C, et al. Anomalous electrical conductivity of nanosheaves of CeO2. Chem Mater, 2009, 21: 1182-1186??
[14]  28 Zhang F, Wong S S. Ambient large-scale template-mediated synthesis of high-aspect ratio single-crystalline, chemically doped rare-earthphosphate nanowires for bioimaging. ACS Nano, 2010, 4: 99-112??
[15]  29 Liu K, You H P, Jia G, et al. Hierarchically nanostructured coordination polymer: Facile and rapid fabrication and tunable morphologies.Cryst Growth Des, 2010, 10: 790-797??
[16]  1 Min Y, Akbulut M, Kristiansen K, et al. The role of interparticle and external forces in nanoparticle assembly. Nat Mater, 2008, 7:527-538??
[17]  2 Wang D, Lieber C M. Inorganic materials: Nanocrystals branch out. Nat Mater, 2003, 2: 355-356??
[18]  3 Nguyen T D, Dinh C T, Do T O. Shape- and size-controlled synthesis of monoclinic ErOOH and cubic Er2O3 from micro- to nanostructuresand their upconversion luminescence. ACS Nano, 2010, 4: 2263-2273??
[19]  4 Jang S Y, Song Y M, Kim H S, et al. Three synthetic routes to single-crystalline PbS nanowires with controlled growth direction and theirelectrical transport properties. ACS Nano, 2010, 4: 2391-2401??
[20]  5 Gao J H, Gu H W, Xu B. Multifunctional magnetic nanoparticles: Design, synthesis, and biomedical applications. Acc Chem Res, 2009,42: 1097-1107??
[21]  6 Xiong Y J, Wiley B J, Xia Y N. Nanocrystals with unconventional shapes—a class of promising catalysts. Angew Chem Int Ed, 2007, 46:7157-7159??
[22]  7 Lu X B, Wen Z H, Li J H. Hydroxyl-containing antimony oxide bromide nanorods combined with chitosan for biosensors. Biomaterials,2006, 27: 5740-5747??
[23]  8 Li J H, Zhang J Z. Optical property and applications of hybrid semiconductor nanomaterials. Coordin Chem Rev, 2009, 253: 3015-3041??
[24]  15 Zhou J, Zhao H W, Li L D, et al. One-step synthesis and flame retardancy of sheaf-like microcrystal antimony oxychloride. J NanosciNanotech, 2011 (in press)
[25]  16 Tang J, Alivisatos A P. Crystal splitting in the growth of Bi2S3. Nano Lett, 2006, 6: 2701-2706??
[26]  21 He J H, Han M, Shen X P, et al. Crystal hierarchically splitting in growth of BaWO4 in positive cat-anionic microemulsion. J CrystGrowth, 2008, 310: 4581-4586
[27]  24 Ota J, Roy P, Srivastava S K, et al. Morphology evolution of Sb2S3 under hydrothermal conditions: Flowerlike structure to nanorods. CrystGrowth Des, 2008, 8: 2019-2023
[28]  25 Zhang M, Xu X D, Zhang M L. Hydrothermal synthesis of sheaf-like CuO via ionic liquids. Mater Lett, 2008, 62: 385-388??
[29]  26 Pan Q T, Huang K, Ni S B, et al. Synthesis of sheaf-like CuO from aqueous solution and their application in lithium-ion batteries. J AlloysComp, 2009, 484: 322-326

Full-Text

Contact Us

service@oalib.com

QQ:3279437679

WhatsApp +8615387084133