全部 标题 作者
关键词 摘要

OALib Journal期刊
ISSN: 2333-9721
费用:99美元

查看量下载量

相关文章

更多...

山楂叶有效成分提取工艺优化及抗氧化活性研究

DOI: 10.11869/j.issn.100-8551.2015.08.1547, PP. 1547-1558

Keywords: 山楂叶,总黄酮,超声波,响应面设计,抗氧化

Full-Text   Cite this paper   Add to My Lib

Abstract:

本试验以山楂叶为研究对象,选取乙醇体积分数、料液比、提取时间、提取温度为自变量,总黄酮得率为响应值,进行四因素三水平的Box-Benhnken试验。利用响应面分析法优化山楂叶总黄酮超声提取工艺,并对山楂叶总黄酮清除DPPH自由基、ABTS自由基能力及其还原力进行探讨。结果表明,超声波辅助乙醇提取山楂叶总黄酮的最佳工艺条件为乙醇体积分数70%,料液比1:35,提取时间39min,提取温度72℃,在此工艺条件下总黄酮得率预测值为29.198mg·g-1,实测值为28.991mg·g-1,与理论预测值的相对误差仅为0.71%。山楂叶总黄酮清除DPPH自由基和ABTS自由基的半抑制浓度(IC50)分别为718.96μg·mL-1和64.43μg·mL-1,而且对Fe3+具有一定的还原能力。试验结果表明,山楂叶总黄酮具有一定的抗氧化活性。本研究为山楂叶功能成分的进一步开发利用提供了科学依据和技术参考。

References

[1]  Roberta R, Pellegrini N, Proteggente A. Antioxidant activity applying an improved ABTS radical cation decolorization assay [J]. Free Radical Biology and Medicine, 1999,26(9/10):1231-1237
[2]  Benzie I F F, Strain J J. The ferric reducing ability of plasma (FRAP) as a measure of "antioxidant power": the FRAP assay[J]. Analytical Biochemistry, 1996,239(1):70-76
[3]  冯进,曾晓雄,李春阳.响应面法优化蓝莓叶多酚提取工艺[J].食品科学,2013,34(4): 59-64
[4]  王昌涛,孙啸涛,周雪.响应面分析法优化雪灵芝黄酮提取工艺[J].食品科学,2013,34(14):91-95
[5]  Yang L, Jiang J G, Li W F. Optimum extraction process of polyphenols from the bark of Phyllanthus emblica L. based on the response surface methodology[J]. Journal of Separation Science,2009,32(9):1437-1444
[6]  李珍,哈益明,李安,李伟明,王锋,李庆鹏.响应面优化苹果皮渣多酚超声提取工艺研究[J].中国农业科学,2013,46(21):4569-4577
[7]  Yue T, Shao D, Yuan Y, Wang Z L, Qiang C Y. Ultrasound-assisted extraction, HPLC analysis, and antioxidant activity of polyphenols from unripe apple[J]. Journal of Separation Science,2012,35(16):2138-2145
[8]  李芳亮,高杨,王锐,孙彦芳,杨腾飞.响应面优化微波辅助提取糜米多糖工艺[J].食品科学,2012,33(20):46-50
[9]  张群飞,徐大纶,杨文鸽.响应面法优化碱性蛋白酶酶解虾籽的工艺条件[J].核农学报,2014,28(5):876-882
[10]  岳瑞雪,孙健,钮福祥,徐飞,朱红.响应面分析法优化甘薯乙醇发酵条件[J].核农学报,2014,28(8):1400-1406
[11]  Sin H N, Yusof S, Abdul Hamid N S. Optimization of hot water extraction for sapodilla juice using response surface methodology[J].Journal of Food Engineering,2006,74(3):352-358
[12]  Dehghan-Shoar Z, Hardacre A K, Meerdink G, Brennan C. Lycopene extraction from extruded products containing tomato skin[J].International Journal of Food Science & Technology,2011,46(2):365-371
[13]  Yi C, Shi J, Xue S J, Jiang Y M, Li D. Effects of supercritical fluid extraction parameters on lycopene yield and antioxidant activity[J].Food Chemistry,2009, 113(4):1088-1094
[14]  施红林,黄琦,褚沈佳.响应面分析法优化山楂叶中黄酮的提取工艺[J].浙江科技学院学报,2014,26(3):165-171
[15]  杨云.中药化学成分提取手册[M].北京:中国中医药出版社,1998
[16]  Sánchez-Moreno C. Review: Methods used to evaluate the free radical scavenging activity in foods and biological systems [J]. Food Science and Technology International, 2002, 8(3): 121-137
[17]  温建丰,杨文鸽,徐大纶.响应面法优化花蟹肉制备抗氧化肽的酶解工艺[J].核农学报,2013,27(12):1881-1886
[18]  姜少娟,马养民,孔东宁,史清华,傅建熙.超声波法提取沙棘果渣中总黄酮的最佳工艺研究[J].西北农林科技大学学报:自然科学版,2006,34(10):184-188
[19]  吴华勇,黄赣辉,顾振宇,董婧,余飞.响应曲面法优化竹叶总黄酮的提取工艺研究[J].食品科学,2008,29(11):196-200
[20]  周海旭,高晗,曲良苗,李忠海.响应面法优化山楂叶中黄酮提取工艺[J].河南农业大学学报,2011,45(6):712-715
[21]  刘通,文连奎.微波辅助提取山楂叶黄酮的试验研究[J].农产品加工(学刊),2014,8(5):10-18
[22]  刘荣华,余伯阳,邱声祥,白桂昌. 山楂叶中多元酚类成分抗超氧阴离子活性研究及构效关系[J]. 中国药学杂志,2005,40(14):1066-1069
[23]  叶希韵, 王耀发. 山楂叶总黄酮对血管内皮细胞氧化损伤的保护作用[J]. 中国现代应用药学, 2002, 19(4): 265-268
[24]  汪晓鸣,刘超,曹磊,李珂昕.山楂黄酮提取物对辐照肉糜脂肪氧化的抑制能力[J]. 核农学报,2011,25(3):514-517
[25]  Kook S H, Son Y O, Jang Y S. Inhibition of c-Jun N-terminal kinase sensitizes tumor cells to flavonoid-induced apoptosis through down-regulation of JunD[J]. Toxicology and Applied Pharmacology, 2008,227(3):468-476
[26]  王军妮,黄艳红,牟志美,王彦文.植物次生代谢物黄酮类化合物的研究进展[J]. 蚕业科学,2007,33(3):499-505
[27]  吕德国,李志霞,鲁巍巍,秦嗣军.山楂叶黄酮提取工艺优化及周年积累动态和分布特性的研究[J].吉林农业大学学报,2010,32(3):271-276
[28]  徐怀德,闫宁环,陈伟,刘丽芳.黑莓原花青素超声波辅助提取优化及抗氧化性研究[J]. 农业工程学报,2008,24(2):264-269
[29]  Pan G, Yu G, Zhu C, Qiao J. Optimization of ultrasound-assisted extraction (UAE) of flavonoids compounds (FC) from hawthorn seed (HS)[J]. Ultrasonics Sonochemistry, 2012,19(3):486-490
[30]  董华强,宁正祥,崔志新,李琳,于立静,林丽超.微波辅助提取多穗柯嫩叶黄酮工艺研究[J]. 农业工程学报,2007,23(2):213-217
[31]  梁艳,应苗苗,吕英华,陆仙英,张英.微波辅助提取仙人掌多糖的工艺研究[J].农业工程学报,2006,22(7):159-162
[32]  王文昕,董全.响应面法优化超声辅助提取花生红衣多酚工艺[J].食品科学,2012,33(22):1-5
[33]  Wang J, Sun B, Cao Y, Tian Y, Li X. Optimization of ultrasound-assisted extraction of phenolic compounds from wheat bran [J]. Food Chemistry,2008, 106(2):804-810
[34]  Zhang H F, Yang X H, Zhao L D. Ultrasonic-assisted extraction of epimedin C from fresh leaves of Epimedium and extraction mechanism[J].Innovative Food Science & Emerging Technologies,2009,10(1):54-60
[35]  Zhang Q A, Zhang Z Q, Yue X F. Response surface optimization of ultrasound-assisted oil extraction from autoclaved almond powder[J]. Food Chemistry,2009,116(2):513-518
[36]  蔡为荣,顾小红,汤坚.仙人掌皮黄酮提取工艺优化[J].农业工程学报,2008,24(6):299-303
[37]  田东,袁其朋,孙新晓,申晓琳.响应面法优化多粘菌素 B 的发酵条件[J].中国农学通报,2010,26(15):53-57
[38]  Herald T J, Gadgil P, Tilley M. High-throughput micro plate assays for screening flavonoid content and DPPH-scavenging activity in sorghum bran and flour [J]. Journal of the Science of Food and Agriculture,2012,92(11):2326-2331
[39]  Molan A L, Flanagan J, Wei W. Selenium-containing green tea has higher antioxidant and prebiotic activities than regular green tea [J]. Food Chemistry, 2009,114(3):829-835

Full-Text

Contact Us

service@oalib.com

QQ:3279437679

WhatsApp +8615387084133