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核农学报  2013 

加压溶剂萃取法提取山楂中黄酮物质的工艺研究

DOI: 10.11869/hnxb.2013.11.1709, PP. 1709-1716

Keywords: 山楂,加压溶剂萃取,总黄酮,正交试验

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Abstract:

为优化加压溶剂萃取方法提取山楂总黄酮的工艺,采用单因素和正交试验,考察了提取温度,提取时间,循环次数,乙醇浓度对山楂中黄酮提取效果的影响。研究表明:加压溶剂萃取方法提取山楂黄酮的最佳工艺条件为提取温度80℃,提取时间5min,循环3次,乙醇浓度50%。在该条件下山楂黄酮最高提取率为4.99%,相对标准偏差为1.01%。加压溶剂萃取方法提取率明显高于超临界提取法和微波提取法,该方法所用试剂少,提取时间短,提取率高,用于黄酮等天然产物提取的前景广阔。

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