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活塞圆筒装置压力盘样品组装的温度测定和热结构分析

DOI: 10.11858/gywlxb.2014.03.002, PP. 262-272

Keywords: 活塞圆筒,尖晶石反应测温法,双热电偶法,热梯度,热结构

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Abstract:

活塞圆筒是目前使用最广泛的固体介质高温高压装置,样品组装方式和组装件的材料类型决定了高压腔体内部的热结构特征。在0.5、1.0、1.5GPa压力下、800~1400℃范围内,采用改进的双热电偶法、尖晶石反应测温法对QUICKpress型活塞圆筒的13mm压力盘的样品组装进行了温度测定,通过获得的实验数据并结合傅里叶热传导模拟结果进行了热结构分析。实验结果表明:(1)热峰位置均位于有效石墨炉中心以下,即靠近钢塞一侧,20℃温差范围的热点区轴向分布区域大小介于2.8~5.2mm,其热梯度为7.7~13.0℃/mm,而非热点区热梯度为42~83℃/mm;(2)随着温度或压力升高,热峰倾向于朝有效石墨炉中心靠拢,同时伴随着炉内热梯度增大和热点区变小,温度的影响更为显著。还对活塞圆筒压力组装的热结构的影响因素及相关问题进行了探讨。

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