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OALib Journal期刊
ISSN: 2333-9721
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锌粉促进三组分“一锅法”合成新型氨基甲酸酯有机化学
DOI: 10.6023/cjoc201402040, PP. 1588-1594
Keywords: 氨基甲酸酯,锌粉,一锅法,三组分,合成
Abstract:
在金属锌的促进下，以醛、溴代烃和异氰酸酯为原料，THF为溶剂，室温、非催化条件下，通过三组分“一锅法”反应合成了一系列新型的氨基甲酸酯类化合物.该方法具有反应条件温和、操作简单、产率高、原料易得、反应迅速的特点.通过1HNMR，13CNMR，IR，HRMS和元素分析对产物结构进行了表征.
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