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OALib Journal期刊
ISSN: 2333-9721
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新型N-酰基-7-甲氧基-苯并[4,5]噻唑并[2,3-c][1,2,4]三唑-3(2H)-硫酮的合成及其除草活性有机化学
DOI: 10.6023/cjoc201308001, PP. 419-423
Keywords: N-酰基-7-甲氧基苯并[4,5]噻唑并[2,3-c][1,2,4]三唑-32H-硫酮,合成,除草活性
Abstract:
为了寻找新的含苯并噻唑稠杂环农药先导化合物，以2-氨基-6-甲氧基苯并噻唑为起始原料，经肼化、环化和酰基化反应，合成出了14个N-酰基-7-甲氧基苯并[4，5]噻唑并[2，3-c][1，2，4]三唑-3（2H）-硫酮，并利用1HNMR，ESI-MS及元素分析对其结构进行表征.对目标化合物进行初步的除草活性筛选，实验结果表明：在浓度为200mg/L时，大部分化合物对黄瓜（Cucumissativus）、小麦（Triticumaestivum）、高粱（Sorghumvulgare）、萝卜（Raphanussativus）、油菜（Brassicacampestris）和稗草（Echinochloacrusgalli）的根和茎的抑制率在85%以上.
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