This work describes an alternative method based on GC/MS technique with SCAN-ion approach for speciation of hydrocarbons contained in soil gas matrices and sampled on solid sorbent tubes (coconut shell charcoal).
References
[1]
Mayer, C.L. (In Press) Guidance Document for Soil-Gas Surveying, Prepared under EPA EMSL-LV Contract n. 68033245. Lockheed Engineering and Sciences Company, Las Vegas.
[2]
Cambiaghi, M., Cogliati, N. and Maspero, M. (2009) Idrocarburi e analisi di rischio: problemi e interpretazioni. Acqua & Aria, 5, 18-23.
[3]
Department of Environmental Protection (2004) Method for the Determination of Volatile Petroleum Hydrocarbons (VPH), Revision 1.1. Department of Environmental Protection, Massachusetts
[4]
Department of Environmental Protection (2004) Method for the Determination of Extractable Petroleum Hydrocarbons (EPH), Revision 1.1. Department of Environmental Protection, Massachusetts.
[5]
Department of Environmental Protection (2009) Method for Determination of Air-Phase Petroleum Hydrocarbon (APH), Final Revision 1. Department of Environmental Protection, Massachusetts.
[6]
EURACHEM (1998) The Fitness for Purpose of Analytical Methods—A Laboratory Guide to Method Validation and Related Topics. EURACHEM Guide, 22.
[7]
UNI EN 13649-2002. Emissioni da sorgente fissa—Determinazione della concentrazione in massa di singoli composti organici in forma gassosa. Metodo mediante carboni attivi e desorbimento con solvente; §7 Procedimento analitico, §§ 7.1. Desorbimento del campione.
[8]
EPA (1999) Compendium Method TO-15.
[9]
EURACHEM-CITAC Guide (2011) Quantifying Uncertainty in Analytical Measurement, Third Edition.
