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Molbank 2013
N-(2-Chloro-5-cyanophenyl)-4,4,4-trifluorobutanamideDOI: 10.3390/M803 Keywords: N-(2-chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide, propylphosphonic anhydride, 4,4,4-trifluorobutanoic acid, 2-amino-4-chlorobenzonitrile. Abstract: N-(2-Chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide ( 3) was synthesized by reacting 4,4,4-trifluorobutanoic acid ( 1) with 2-amino-4-chlorobenzonitrile ( 2) in the presence of triethylamine and propylphosphonic anhydride in ethyl acetate. Character-ization of the compound was done by IR, 1H-NMR, 13C-NMR, LC-MS and CHN analysis.
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