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Heterocyclic Letters 2012
SYNTHESIS, CHARACTERIZATION OF SOME MANNICH BASE NEW 1, 3, 4- OXADIAZOLE-2-THIONE DERIVATIVES SYNTHESIS, Charakterisierung einiger Mannichbase NEU 1, 3, 4 - Oxadiazol-2-thion DERIVATEDOI: september 30,2011. Keywords: 1 , 3 , 4 oxadiazole, Mannich reaction, Thiol, Synthesis, Characterization. Abstract: Two new oxadiazole compounds 3,3 -[methylin-bis(1,4-phenyline-iminomethyline]-bis-(5- phenyl-1,3,4-oxadiazol)-2,3(H)-thione and 5-phenyl3-[4-(5-phenyl-1,3,4-oxadiazole-3yl) methyl]amino}phenyl)amino]methyl1,3,4-oxadiazolidine-2-thione thiooxamethane have been synthesized. The reaction was done in pH= 7 and in presences of amin molecules by Mannich reaction. The structures of the compounds were characterized by FT-IR,13 C NMR and 1H NMR techniques.
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