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色谱  1999 

Study on the Analytical Method of Methyl-Parathion and Phoxim in Methyl-Parathion, Phoxim and Cypermethrin Mixed Formulation
氯甲辛三元混合制剂中甲基对硫磷和辛硫磷的分析方法研究

Keywords: high performance liquid chromatography,methyl-parathion,phoxim
氯甲辛
,杀虫剂,HPLC,甲基对硫磷,辛硫磷,测定

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Abstract:

This paper describes an HPLC method to simultaneously determine methyl-parathion and phoxim in mixed formulation of methyl-parathion, phoxim and cypermethrin. A C, column was used. The mobile phase was V(MeOH): V(H2O) = 70: 30, Methyl-parathion and phoxim were monitored at 254 urn or 280urn by UV detector. The average recoveries were 99. 8% and 99. 9% for methyl-parathion and phoxim respectively. The linearity of detector response vs concentration was calibrated in the concentration ranges from 0. 1746 to 1. 091 g/L for methyl-parathion and from 0. 1927 to 1. 205 g/L for phoxim.

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