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色谱  1999 

Analysis of HPLC of Isomers of Nitrotoluene and Nitrobenzoic Acid
硝基甲苯与硝基苯甲酸异构体的高效液相色谱法分析

Keywords: high performance liquid chromatography,isomer,nitrotoluene,nitrobenzoic acid
异构体
,硝基甲苯,硝基苯甲酸,分离,HPLC

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Abstract:

Nitrotoluene and nitrobenzoic acid isomers were separated completely in less than 10 minutes by Kromasil C18 (200 mm x 4.6 mm i.d.), when V(CH3OH):V(H2O):V(THF) = 55:44:1 with beta-CD of 0.02 mol/L at flow rate of 2.0 mL/min (former 4 min) and 2.6 mL/min (later 6 min). Detector of UV-254 at 0.04 AUFS was used.

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