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色谱  1998 

Determination of Formaldehyde in Indoor Air by Gas Chromatography
居室空气中甲醛的气相色谱法分析

Keywords: gas chromatography with derivatization,indoor air,formaldehyde
衍生气相色谱法
,甲醛,居室空气,GC

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Abstract:

Formaldehyde in indoor air was collected by water, derivatized with 2,4 dinitrophenylhydrazine and extracted by cyclohexane. The sample was separated on an OV 17 and QF 1 mixed chromatographic column and determined by electron capture detector. The detection limit was 0.02mg/L(solution), the minimum detectable concentration was 0.01mg/m 3 while 10L indoor air was collected. The results show that this is a rapid and sensitive method with less interferences and fairly good precision. The recoveries were 71.0% 90 4% and coefficients of variation were 4.1% 6.5%. The development of this method has made a reliable methodological foundation for the determination of formaldehyde in indoor air.

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