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色谱 1998
Determination of Formaldehyde in Indoor Air by Gas Chromatography
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Abstract:
Formaldehyde in indoor air was collected by water, derivatized with 2,4 dinitrophenylhydrazine and extracted by cyclohexane. The sample was separated on an OV 17 and QF 1 mixed chromatographic column and determined by electron capture detector. The detection limit was 0.02mg/L(solution), the minimum detectable concentration was 0.01mg/m 3 while 10L indoor air was collected. The results show that this is a rapid and sensitive method with less interferences and fairly good precision. The recoveries were 71.0% 90 4% and coefficients of variation were 4.1% 6.5%. The development of this method has made a reliable methodological foundation for the determination of formaldehyde in indoor air.