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波谱学杂志 2007
NMR Studies on Glycosyl Guanidines Containing Arylthiazol
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Abstract:
Four new tetraacetyl galactosylguanidines were synthesized and characterized by NMR spectroscopy. The ^1H and ^13C NMR chemical shifts of these compounds were assigned using both 1D and 2D techniques, including ^1H NMR, ^13C NMR,^1H-^1H COSY, gHMQC, gHMBC and NOESY. The NMR data showed that all galactosyl had the same configuration of fl-anomer. The spectral characteristics of the compounds were analyzed and compared.