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OALib Journal期刊
ISSN: 2333-9721
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一种利用梯度光掩模制备梯度表面的简便方法
DOI: 10.3724/SP.J.1105.2011.10127, PP. 509-515
Keywords: 梯度光掩模,受限光催化氧化反应,光接枝,聚合物梯度表面,丙烯酰胺,丙烯酸
Abstract:
以自制杂化双向拉伸聚丙烯/氧化硅（BOPP/SiOx）有机/无机杂化膜为基材，由喷墨打印机直接在杂化膜表面打印色阶图案，制备出对紫外光强度呈梯度透过的梯度光掩模；通过此掩模控制，在双向拉伸聚丙烯（BOPP）和聚对苯二甲酸乙二醇酯（PET）表面实施受限光催化氧化（CPO）光感应羟基化反应、受限光接枝丙烯酸（AA）以及表面沉淀紫外光接枝丙烯酰胺（AM）聚合反应.全反射红外光谱（ATRFTIR）、X射线光电子能谱（XPS）、水接触角、荧光显微镜及扫描电镜（SEM）分析表明，分别得到表面能、接枝层厚度及接枝链密度呈梯度分布的功能性梯度表面.
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