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OALib Journal期刊
ISSN: 2333-9721
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双壳微纳米相变胶囊制备影响因素的研究
Keywords: 有机高分子材料,双壳微纳米相变胶囊,细乳液界面聚合法,形貌,粒径,影响因素
Abstract:
？以相变材料为芯材、聚苯乙烯为内壳、亲水性壳聚糖为外壳、以十二烷基硫酸钠为乳化剂、十六烷为助乳化剂、偶氮二异丁腈为引发剂,壳核比为1∶1,用细乳液界面聚合法制备双壳微纳米相变胶囊,用ft-ir、dsc、sem、lpsa对其表征,研究了芯材种类、乳化剂用量、助乳化剂用量、引发剂用量、超声乳化时间、搅拌速度等对双壳微纳米相变胶囊形貌的影响。结果表明,双壳微纳米相变胶囊形貌受到芯材种类、乳化剂用量、助乳化剂用量以及引发剂用量的影响较大,也与超声乳化时间和搅拌速度有关,并得到相应最佳工艺参数。
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