TAMASSO M,PEREGO G,NOTARI B.Preparation of porous crystallinesynthetic material comprised of silicon and titanium oxide[P].US Patent,4410501,1983. [2]THANGARAJ A,EAPEN M J,SIVASANKER S,et al.Studies on the synthesis of titanium silicalite TS-1[J].Zeolites,1992,12(8):943-950. [3]李明丰,郭新闻,王祥生.以de-[B]ZSM-5为母体合成Ti-ZSM-5[J].催化学报,1997,18(4):269-270.LI Mingfeng,GUO Xinwen,WANG Xiangsheng.Chin J Catal(in Chinese),1997,18(4):269-270. [4]郭新闻,李钢,王祥生.钛硅沸石UV-Vis谱的研究[J].大连理工学报,1998,38(3):359-362.GUO Xinwen,LI Gang,WANG Xiangsheng.J Dilian Univ Tech(in Chinese),1998,38(3):359-362. [5]TUEL A.Crystallization of titanium silicalite-1(TS-1)from gels containing[J].Zeolites,1996,16(2/3):108-117. [6]LI Gang,GUO Xinwen,WANG Xiangsheng,et al.Synthesis of tita-nium silicalites in different template systems and their catalytic per-formance[J].Appl Catal A,1999,185(1):11-18. [7]UGUINA M A,SERRANO D P,OVEJERO G,et al.Preparation of TS-1by wetness impregnation amorphous SiO2-TiO2solids:Influence of the synthesis variables[J].Appl Catal,A:General,1995,124(2):391-408. [8]王丽琴,王祥生,郭新闻,等.合成TS-1分子筛的结晶动力学及催化性能研究[J].催化学报,2003,24(2),132-136.WANG Liqin,WANG Xiangsheng,GUO Xinwen.Chin J Catal(in Chinese),2003,24(2):132-136. [9]ZHANG Haijiao,LIU Yueming,WU Haihong,et al.Hydrothermal synthesis of hexamethyleneimine-templated TS-1titanosilicate sup-ported by active seeds[J].Chem.Lett,2006,35(11):1276-1277. [10]XU W Y,DONG J,LI J,WU F.A novel method for the preparation of zeolite ZSM-5[J].J Chem Soc,Chem Commun,1990,10:755-756. [11]MASAHIKO MATSUKATA,NORIKAZU NISHIYAMA,KOREKAZU UEYAMA.Crystallization of FER and MFI zeolites by a vapor-phase transport method[J].Micro Mater,1996,7:109-117. [12]PENG Wu,TAKAYUKI MIYAJI,LIU Yueming,et al.Synthesis of Ti MWW by a dry-gel conversion method[J].Catal Today,2005,99:233-240. [13]TATSUMI T,JAPPAR N.Properties of Ti-beta zeolites synthesized by a dry gel conversion method and hydrothermal method[J].J Phys Chem B,1998,102(37):7126-7131. [14]张小明,丁勇,彭志光,等.一种钛硅分子筛的制备方法[P].CN Patent1327947,2001.ZHANG Xiaoming,DING Yong,PENG Zhiguang,et al.A preparation method of titanium silicalite zeolite[P].CN Patent1327947,2001. [15]揭嘉,吴保林,周继承.TS-1合成时晶种与模板剂的协同导向作用[J].精细化工中间体,2001,31(2):18-21.JIE Jia,WU Baolin,ZHOU Jicheng.Fine Chem Inter(in Chinese),2001,31(2):18-21. [16]徐如人,庞文琴.无机合成与制备化学[M].北京:高等教育出版社,2002:429-430.XU Ruren,PAN Wenqin.Inorganic Synthesis and Preparative Chemistry(in Chinese).Beijing:Higher Education Press,2002:429-430. [17]XIA Q H,TATSUMI T.Crystallization kinetics of nanosized Tiβzeolites with high oxidation activity by a dry-gel conversion technique[J].Mater Chem Phys,2005,89:89-98.